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The Analysis of Silicate Ad Carbonate Rocks Volume 302-307

The Analysis of Silicate Ad Carbonate Rocks Volume 302-307


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This historic book may have numerous typos and missing text. Purchasers can download a free scanned copy of the original book (without typos) from the publisher. Not indexed. Not illustrated. 1907 Excerpt: ...precipitation by ammonium sulphide, and contamination by other bodies. Because of the small amounts in question these errors may be relatively enormous, and they can not be depended on to balance each other. Therefore, it would be an advance if the total manganese could be determined in a separate portion of the sample, and in the main portion only that part which is weighed with the magnesium pyrophosphate, and this only as a correction to the magnesia. This course is readily feasible with carbonate rocks, which can usually be brought into a fit state in a few minutes without a fusion or the separation of silica. With silicate rocks more labor is involved, but the determination itself is very accurately performed by colorimetry, as in the case of carbonates. The preliminary treatment consists in decomposing a gram or half a gram of the rock powder in a small platinum dish or capacious crucible (placed in the radiator shown in fig. 2, p. 29) with hydrofluoric and sulphuric acids till all is disintegrated. The hydrofluoric acid is then to be driven off by repeated evaporations with small portions of sulphuric acid, after which nitric acid free from chlorine is added, together with water, and as much of the residue is brought into solution as possible. What remains insoluble is usually barium and calcium sulphates. This is filtered off on a small filter, the filtrate is caught in a small beaker or flask, and the manganese determined as in the following paragraphs. b. COLORIMETRIC DETERMINATION OF MANGANESE BY AMMONIUM FERSULPHATE.O This method has the advantage over that by lead peroxide in that, unless chlorides happen to be in the solution, no filtration is necessary. Two solutions are needed, one of silver nitrate containing 2 grams of the salt to the lite...


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Product Details
  • ISBN-13: 9781130293173
  • Publisher: Rarebooksclub.com
  • Publisher Imprint: Rarebooksclub.com
  • Height: 246 mm
  • No of Pages: 88
  • Spine Width: 5 mm
  • Width: 189 mm
  • ISBN-10: 1130293173
  • Publisher Date: 01 Mar 2012
  • Binding: Paperback
  • Language: English
  • Returnable: N
  • Weight: 172 gr


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