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Home > Biographies & Memoire > Biography and non-fiction prose > Anthologies: general > The Analysis of Silicate and Carbonate Rocks Volume 697-701
The Analysis of Silicate and Carbonate Rocks Volume 697-701

The Analysis of Silicate and Carbonate Rocks Volume 697-701


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This historic book may have numerous typos and missing text. Purchasers can download a free scanned copy of the original book (without typos) from the publisher. Not indexed. Not illustrated. 1919 Excerpt: ...methods have been compared by O. Brunck,1 who finds that duplicates by any one of them show better agreement than by the oxide method. Brief descriptions of them are therefore given below, as well as of the volumetric method. It is to be said, however, regarding Brunck's determination of calcium as the oxide, that no such variations as those reported by him are ever obtained in the Survey laboratory. Duplicates by that method agree as well as his by the other methods. His high and varying results by the oxide method are probably to be attributed to the employment of a vertical instead of an inclined flame. The complete conversion of the oxide to sulphate or to fluoride by treat 1 Zeitschr. anal. Chemie, vol. 45, 1906, p. 77. ment with sulphuric or hydrofluoric acid is, in my opinion, based on experience with the conversion of lead chloride to sulphate, by no means easily brought about. There will always be a tendency, where an insoluble compound is at once produced by action of one of the acids in question, for some of the original compound to be protected from conversion to the salt, even after two or more evaporations with fresh portions of acid. It is further doubtful if the loss in weight of the crucible during blast ignition of the lime is really as great as he thinks. It is well known that barium oxide attacks platinum strongly when heated in contact with it, and it is certain that lime does so to a less but appreciable extent. That it does can be demonstrated readily by dissolving in hydrochloric acid lime that has been blasted in platinum for half an hour and precipitating and weighing the dissolved platinum. The amount recovered will nearly and sometimes quite equal the loss in weight of the crucible itself. b. VOLUMETRIC METHOD. The washed oxalate...


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Product Details
  • ISBN-13: 9781156104170
  • Publisher: Rarebooksclub.com
  • Publisher Imprint: Rarebooksclub.com
  • Height: 246 mm
  • No of Pages: 130
  • Spine Width: 7 mm
  • Width: 189 mm
  • ISBN-10: 1156104173
  • Publisher Date: 01 May 2012
  • Binding: Paperback
  • Language: English
  • Returnable: N
  • Weight: 245 gr


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