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Qualitative Analysis Volume 70; Quantitative Analysis

Qualitative Analysis Volume 70; Quantitative Analysis


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Purchase of this book includes free trial access to www.million-books.com where you can read more than a million books for free. This is an OCR edition with typos. Excerpt from book: coal gas) was measured in the burette, and an excess of air added. Volume of gas taken = 14.2 c. c. Volume of gas ] air = 97.6 c. c. Volume after explosion = 74.2 c. c. Therefore, contraction C = 97.6 ? 74.2 = 23.4 c. c. After absorption by KOH, volume = 68.2 c. c. Therefore, C' = 74.2-68.2 = 6.0 c. c. Hence, volume of H in 14.2 c. c. of the gas = ](23.4-12) = 7.6 C.C., and volume of CHt in 14.2 c. c. of the gas = 6.0 c.c., and volume of N in 14.2 c.c. of the gas = 14.2-(7.6+ 6.0) = 0.6 c. c. Calculating the percentage as in the previous instance, 7.6X8.6 14.2 6 X 86.6 14.2 .6X86.6 In cases where the gas under analysis contains a relatively large proportion of nitrogen, as, for example, in the case of producer gas or blast-furnace gases, the addition of air would dilute the gas to such an extent as to render it non- combustible. Under these circumstances, therefore, either oxygen must be substituted for air, or else, after sufficient air has been added to furnish the requisite amount of oxygen, a few cubic centimeters of electrolytic gas may be added to the mixture. The electrolytic gas for this purpose may be generated in the pipette described in Art. 41, and then transferred to the mercury-explosion pipette. = 36.5 of marsh gas = 3.6 of nitrogen THE NITROMETER AND GASVOLUMETER 5O. The nitrometer and the (tasvolumeter, which were invented by Lunge, simplify gas analyses very much, and may be used for many determinations where gases are evolved. They are made in several forms; but only those forms that have given the best satisfaction are described.The form of gasvolumeter described was designed by Jopp. The nitrometer, Fig. 17 (a), consists of two glass tubes c, f, connected by a rubber tube. The tube e is provided with a three-way sto...


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Product Details
  • ISBN-13: 9780217538237
  • Publisher: Rarebooksclub.com
  • Publisher Imprint: Rarebooksclub.com
  • Height: 246 mm
  • No of Pages: 136
  • Spine Width: 7 mm
  • Width: 189 mm
  • ISBN-10: 0217538231
  • Publisher Date: 10 May 2012
  • Binding: Paperback
  • Language: English
  • Returnable: N
  • Weight: 254 gr


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