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Home > Medicine & Health Science textbooks > Medical specialties, branches of medicine > Pharmacology > Metodo per la stima simultanea di glucosamina e acidi boswellici
Metodo per la stima simultanea di glucosamina e acidi boswellici

Metodo per la stima simultanea di glucosamina e acidi boswellici


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About the Book

Obiettivo: L'obiettivo è quello di sviluppare e convalidare un metodo HPTLC semplice, accurato, sensibile e rapido per la stima simultanea della glucosamina (GLU) e degli acidi β-boswellici (BA) nella loro forma farmaceutica combinata in compresse. Lavoro sperimentale: Nel metodo HPTLC, la separazione cromatografica è stata effettuata su una piastra TLC pre-rivestita con gel di silice 60F254 utilizzando la fase mobile A, toluene-etilacetato (2,5:1,5 v/v) per 11-KBA e A-11-KBA, scansionando la piastra a 260 nm [scansione 1] e la fase mobile B, 1-butanolo-acqua-acido acetico glaciale (3:1:1, v/v/v) per GLU, derivatizzando la piastra con reagente ninidrina e scansionando la piastra a 485 nm [scansione 2]. Risultati: Il metodo HPTLC è risultato lineare nell'intervallo 6250-31250, 300-1500 e 150-750 ng/banda rispettivamente per GLU, 11-KBA e A-11-KBA.Con questo metodo, la % RSD della determinazione del dosaggio di entrambi i farmaci è risultata inferiore al 2,0 e la % media di recupero è risultata compresa tra il 98 e il 101%. Conclusione: il metodo è risultato preciso, poiché la % RSD del dosaggio in tutti i casi era inferiore al 2,0. L'elevata percentuale di recupero ottenuta con questo metodo indica che il metodo è accurato. Non si è verificata alcuna interferenza da parte di eccipienti nella determinazione dei farmaci nelle compresse.


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Product Details
  • ISBN-13: 9786202357418
  • Publisher: Edizioni Sapienza
  • Publisher Imprint: Edizioni Sapienza
  • Height: 229 mm
  • No of Pages: 84
  • Spine Width: 5 mm
  • Width: 152 mm
  • ISBN-10: 620235741X
  • Publisher Date: 04 Aug 2025
  • Binding: Paperback
  • Language: Italian
  • Returnable: N
  • Weight: 177 gr


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