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Synthesis of Polycyclic Aromatics With Unusual Architectures

Synthesis of Polycyclic Aromatics With Unusual Architectures


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About the Book

The C2-C6 Schmittel cyclization reaction of the benzannulated enyne-allenes provides an efficient synthetic pathway for the construction of a variety of polycyclic aromatics. By starting from truxenone, the cascade cyclization reactions furnished several unusual and congested polycyclic compounds. A new synthetic approach to 2,2′-disubstituted 1,1′- binaphthyls and related compounds was also successfully developed using the benzannulated enediynes as precursors. These 1,1′-binaphthyls derivatives can serve as potential BINOL type ligands. The assembly of the enediynyl precursors from three separate aromatic fragments allows the possibility of placing a variety of functional groups at various positions of the 1,1′-binaphthyl system. A 12-step non-pyrolytic synthetic pathway employing the Schmittel cyclization reactions has been developed, leading to a bowl-shaped polycyclic aromatic hydrocarbon (PAH) having a 54-carbon framework of the surface of C60. Incorporating of sp3-carbons on the 54-carbon framework facilitates the connection of carbon atoms intramolecularly.


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Product Details
  • ISBN-13: 9783639166040
  • Publisher: VDM Verlag
  • Publisher Imprint: VDM Verlag
  • Height: 229 mm
  • No of Pages: 250
  • Spine Width: 14 mm
  • Width: 152 mm
  • ISBN-10: 3639166043
  • Publisher Date: 26 Jul 2009
  • Binding: Paperback
  • Language: English
  • Returnable: N
  • Weight: 421 gr


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