Supported Ionic Liquids
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Supported Ionic Liquids: Fundamentals and Applications

Supported Ionic Liquids: Fundamentals and Applications


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About the Book

This unique book gives a timely overview about the fundamentals and applications of supported ionic liquids in modern organic synthesis. It introduces the concept and synthesis of SILP materials and presents important applications in the field of catalysis (e.g. hydroformylation, hydrogenation, coupling reactions, fine chemical synthesis) as well as energy technology and gas separation. Written by pioneers in the field, this book is an invaluable reference book for organic chemists in academia or industry.

Table of Contents:
Preface INTRODUCTION A Century of Supported Liquids Supported Ionic Liquids Applications in Catalysis Applications in Separation Coating of Heerogeneous Catalysts Monolayers of IL on Surfaces Conclusion PART I: Concept and Building Blocks INTRODUCING IONIC LIQUIDS Introduction Preparation Liquid Range Structures Physical Properties Effects of Ionic Liquids on Chemical Reactions Ionic Liquids as Process Solvents in Industry Summary POROUS INORGANIC MATERIALS AS POTENTIAL SUPPORTS FOR IONIC LIQUIDS Introduction Porous Materials - An Overview Silica-Based Materials - Amorphous Layered Materials Ordered Mesoporous Materials Structured Supports and Monolithic Materials Conclusions SYNTHETIC METHODOLOGIES FOR SUPPORTED IONIC LIQUID MATERIALS Introduction Support Materials Preparation Methods for Supported Ionic Liquids Summary PART II: Synthesis and Properties PORE VOLUME AND SURFACE AREA OF SUPPORTED IONIC LIQUIDS SYSTEMS Example I: [EMIM][NTf2] on Porous Silica Example II: SCILL Catalyst (Commercial Ni catalyst) Coated with [BMIM][OcSO4] TRANSPORT PHENOMENA, EVAPORATION, AND THERMAL STABILITY OF SUPPORTED IONIC LIQUIDS Introduction Diffusion of Gases and Liquids in ILs and Diffusivity of ILs in Gases Thermal Stability and Vapor Pressure of Pure ILs Vapor Pressure and Thermal Decomposition of Supported ILs Outlook IONIC LIQUIDS AT THE GAS-LIQUID AND SOLID-LIQUID INTERFACE - CHARACTERIZATION AND PROPERTIES Introduction Characterization of Ionic Liquid Surfaces by Spectroscopic Techniques Orientation and Properties of Ionic Liquids at the Solid-Liquid Interface Comments SPECTROSCOPY ON SUPPORTED IONIC LIQUIDS NMR-Spectroscopy IR Spectroscopy A PRIORI SELECTION OF THE TYPE OF IONIC LIQUID Introduction and Objective Methods Usage of COSMO-RS to Predict Solubilities in IL Results of Reaction Modeling Perspectives of the A Priori Selection of ILs PART III: Catalytic Applications SUPPORTED IONIC LIQUIDS AS PART OF A BUILDING-BLOCK SYSTEM FOR TAILORED CATALYSTS Introduction Immobilized Catalysts Supported Ionic Liquids The Building Blocks Catalysis in Supported Thin Films of IL Supported Films of IL in Catalysis Advantages and Drawbacks of the Concept Conclusions COUPLING REACTIONS WITH SUPPORTED IONIC LIQUID CATALYSTS Introduction A Short History of Supported Ionic Liquids Properties of SIL Application of SIL in Coupling Reactions Conclusion SELECTIVE HYDROGENATION FOR FINE CHEMICAL SYNTHESIS Introduction Selective Hydrogenation of Alpha,Beta-Unsaturated Aldehydes Asymmetric Hydrogenations over Chiral Metal Complexes Immobilize3d in SILCAs Conclusions HYDROGENATION WITH NANOPARTICLES USING SUPPORTED IONIC LIQUIDS Introduction MNPs Dispersed in ILs: Green Catalysts for Multiphase Reactions MNPs Immobilized on Supported Ionic Liquids: Alternative Materials for Catalytic Reactions Conclusions SOLID CATALYSTS WITH IONIC LIQUID LAYER (SCILL) Introduction Classification of Applications of Ionic Liquids in Heterogeneous Catalysis Preparation and Characterization of the Physical Properties of the SCILL Systems Kinetic Studies with SCILL Catalysts Conclusions and Outlook SUPPORTED IONIC LIQUID PHASE (SILP) MATERIALS IN HYDROFORMYLATION CATALYSIS SILP Materials in Liquid-Phase Hydroformylation Reactions Gas-Phase SILP Hydroformylation Catalysis SILP Combined with scCO2 - Extending the Substrate Range Continuous SILP Gas-Phase Methanol Carbonylation Conclusion and Future Potential ULTRALOW TEMPERATURE WATER-GAS SHIFT REACTION ENABLED BY SUPPORTED IONIC LIQUID PHASE CATALYSTS Introduction to Water-Gas Shift Reaction Challenges SILP Catalyst Development Building-Block Optimization Application-Specific Testing Conclusion BIOCATALYTIC PROCESSES BASED ON SUPPORTED IONIC LIQUIDS Introduction and General Concepts Biocatalysts Based on Supported Ionic Liquid Phases (SILPs) Biocatalysts Based on Covalently Supported Ionic Liquid-Like Phases (SILLPs) Conclusions/Future Trends and Perspectives SUPPORTED IONIC LIQUID PHASE CATALYSTS WITH SUPERCRITICAL FLUID FLOW Introduction SILP Catalysis PART IV: Special Applications PHARMACEUTICALLY ACTIVE SUPPORTED IONIC LIQUIDS Active Pharmaceutical Ingredients in Ionic Liquid Form Solid-Supported Pharmaceuticals Silica Materials for Drug Delivery Factors That Influence the Loading and Release Rate of Drugs SILPs Approach for Drug Delivery Conclusions SUPPORTED PROTIC IONIC LIQUIDS IN POLYMER MEMBRANES FOR ELECTROLYTES OF NONHUMIDIFIED FUEL CELLS Introduction Protic ILs as Electrolytes for Fuel Cells Membrane Fabrication Including PIL and Fuel Cell Operation Proton Conducting Mechanism during Fuel Cell Operation Conclusion GAS SEPARATION USING SUPPORTED IONIC LIQUIDS SILP Materials Supported Ionic Liquid Membranes (SILMs) Conclusion IONIC LIQUIDS ON SURFACES - A PLETHORA OF APPLICATIONS Introduction The Influence of ILs on Solid-State Surfaces Layers of ILs on Solid-State Surfaces Selected Applications Sensors Electrochemical Double Layer Capacitors (Supercapacitors) Dye Sensitized Solar Cells Lubricants Synthesis and Dispersions of Nanoparticles PART V: Outlook OUTLOOK - THE TECHNICAL PROSPECT OF SUPPORTED IONIC LIQUID MATERIALS Competitive Advantage Observability Trialability Compatibility Complexity Perceived Risk

About the Author :
Rasmus Fehrmann is Professor and head of the Centre for Catalysis and Sustainable Chemistry at the Department of Chemistry, Technical University of Denmark (DTU). After obtaining his PhD from DTU he was awarded university candidate- and senior scholarships as well as postdoctoral fellowships at the Institute of Catalysis in Novosibirsk (Russia), Universite de Provence (France), and University of Patras (Greece), before taking up his present appointment. His main scientific achievements fall within the chemistry of sulfuric acid catalysts, environmental catalysis and ionic liquid fundamentals and applications including SLP and SILP technologies. Professor Fehrmann has authored over 130 scientific publications, 20 patent applications, and 400 oral or poster presentations at international conferences, and has been a board member of the Danish National Committee for Chemistry for over a decade. Anders Riisager is Associate Professor at the Centre for Catalysis and Sustainable Chemistry at the Department of Chemistry, Technical University of Denmark (DTU). He studied Chemistry at the University of Copenhagen (Denmark) and obtained his PhD in catalysis from DTU in 2002. Subsequently he acquired a three-year postdoctoral fellowship at RWTH-Aachen/ University of Erlangen-Nuremberg (Germany) followed by a one-year Villum Kann Rasmussen postdoctoral fellowship at DTU, where he developed novel SILP catalysts and processes. He has authored more than 80 scientific publications and 20 patent applications, and received several honors including a nomination for the Degussa European Science-to-Business Award 2006 for SILP materials. His main scientific focus is the development of sustainable ionic liquid catalysis and separation technology. Marco Haumann has been a lecturer at the University of Erlangen-Nuremberg (FAU, Germany) since 2003. He studied Engineering and Chemistry at the universities of Dortmund and Berlin (Germany). After obtaining his PhD in 2001, he spent two years at the universities of Cape Town and Johannesburg (South Africa), developing novel catalysts in collaboration with Sasol Technology Pty Limited. From 2011 to the end of 2012, he was in charge of the establishment of the new FAU Branch Campus in Busan, South Korea. He has authored more than 40 scientific publications and was awarded the Arnold-Eucken prize of the Association of German Engineers (VDI-GVC) in 2011 for his contributions on SILP technology. His main scientific focus is the development of novel supported ionic liquid phase materials for catalysis and separation science.


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Product Details
  • ISBN-13: 9783527324293
  • Publisher: Wiley-VCH Verlag GmbH
  • Publisher Imprint: Blackwell Verlag GmbH
  • Height: 246 mm
  • No of Pages: 496
  • Spine Width: 31 mm
  • Weight: 1225 gr
  • ISBN-10: 3527324291
  • Publisher Date: 22 Jan 2014
  • Binding: Hardback
  • Language: English
  • Returnable: N
  • Sub Title: Fundamentals and Applications
  • Width: 170 mm


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