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Monitoring Iron Mineralization Processes Using Nuclear Magnetic Resonance

Monitoring Iron Mineralization Processes Using Nuclear Magnetic Resonance


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About the Book

Proton nuclear magnetic resonance (NMR) measurements can be used to probe the molecular-scale physical and chemical environment of water in the pore space of geological materials. In geophysics, NMR relaxation measurements are used in to measure water content and estimate permeability in the top 100 m of Earth's surface. The goal of the research presented in this thesis is to determine if NMR can also be used in geophysical applications to monitor iron mineralization processes associated with contaminant remediation. The first part of the research presented in this thesis focuses on understanding the effect of iron mineral form and redox state on the NMR relaxation response of water in geologic material. Laboratory NMR measurements were made on Fe(III)-bearing minerals (ferrihydrite, lepidocrocite, goethite, and hematite), Fe(II)-bearing minerals (siderite, pyrite, and troilite), and a mixed valence iron-bearing mineral (magnetite). The results of these measurements show that the relaxation rate of water is strongly dependent on the mineral form of iron. Shown in the final section of this thesis are results from an experiment exploring temporal changes in the measured NMR relaxation rates during the reaction of ferrihydrite with aqueous Fe(II). These results show that NMR can be used to monitor temporal chemical changes in iron minerals. I conclude that this research shows that NMR indeed has the potential to be used as a tool for monitoring geochemical reactions associated with contaminant remediation.


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Product Details
  • ISBN-13: 9781243609168
  • Publisher: Proquest, Umi Dissertation Publishing
  • Publisher Imprint: Proquest, Umi Dissertation Publishing
  • Height: 246 mm
  • Weight: 336 gr
  • ISBN-10: 1243609168
  • Publisher Date: 01 Sep 2011
  • Binding: Paperback
  • Spine Width: 10 mm
  • Width: 189 mm


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