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Daedalus Volume 43; Proceedings of the American Academy of Arts and Sciences

Daedalus Volume 43; Proceedings of the American Academy of Arts and Sciences


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About the Book

This historic book may have numerous typos and missing text. Purchasers can download a free scanned copy of the original book (without typos) from the publisher. Not indexed. Not illustrated. 1908 Excerpt: ...the blank test may be as long continued as circumstances demand. The solution to be tested is then introduced, either wholly or in aliquot part, which may be determined by weighing or measuring. In the former case we use a side-neck test tube of about 30 c.c. capacity, and weigh to the second decimal place. Unless the amount of arsenic be exceedingly small, it is not necessary to add the whole of the solution, but in that case the volume must be obviously not over 15 c.c, on account of the capacity of the bottle. After introduction of the solution the color appears upon the paper in a few minutes and the deposit reaches its maximum within thirty minutes. The band of color thus obtained is then compared with a set of standard bands. From the amount of arsenic as estimated from the comparison, and the amount of solution from which the band was obtained, the calculation of the arsenic in the entire solution is simple. We are also indebted to the Baker and Adamson Company for a preparation of hydrochloric acid containing a still smaller quantity of arsenic, the use of which will be later explained in the discussion of the absolute delicacy of the method. Standard Color Bands. A standard solution is made by dissolving one gram of re-sublimed arsenious oxide in a small quantity of sodio hydroxide free from arsenic, acidifying with sulphuric acid and making up to one liter with recently boiled water. Of this solution (I) 10 c.c are diluted to a liter with freshly boiled water, giving a solution (II) which contains 0.01 mg. or 10 micromilligrams (mmg.) of arsenious oxide per cubic centimeter. In testing the delicacy of the method we have also prepared solutions containing 1 mmg. (Ill) and 0.1 mmg. (IV) per cubic centimeter. From definite portions of solution II, me...


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Product Details
  • ISBN-13: 9781236008893
  • Publisher: Rarebooksclub.com
  • Publisher Imprint: Rarebooksclub.com
  • Height: 246 mm
  • No of Pages: 172
  • Spine Width: 9 mm
  • Width: 189 mm
  • ISBN-10: 1236008898
  • Publisher Date: 01 May 2012
  • Binding: Paperback
  • Language: English
  • Returnable: N
  • Weight: 318 gr


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