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Methods in Chemical Analysis; Originated or Developed in the Kent Chemical Laboratory of Yale University

Methods in Chemical Analysis; Originated or Developed in the Kent Chemical Laboratory of Yale University


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This historic book may have numerous typos and missing text. Purchasers can download a free scanned copy of the original book (without typos) from the publisher. Not indexed. Not illustrated. 1912 Excerpt: ...before they are oxidized appreciably by atmospheric action. Arsenic, Antimony And Tin. The Determination of Arsenic by Precipitation as Ammonium Magnesium Arsenate and Weighing as Magnesium Pyroar senate. The striking analogy between the phosphates and the arse, nates led Levol to undertake the separation of an ammonium arsenate corresponding to the ammonium magnesium phosphate, the composition of which Berzelius had given. Levol states that ammonium magnesium arsenate of the composition NH4MgAsCV10HsO is obtained by adding a solution of a double ammonium magnesium salt to arsenic acid, that it is a salt possessing about the same degree of solubility in water, in am, moniacal water, and in ammoniacal water containing magnesium salt, as the corresponding phosphate, and that at red heat, after carefully drying, it yields magnesium pyroarsenate. Several sources of error in this process have been pointed out by many investigators. First, the low indications obtained when the pyroarsenate is weighed suggest a loss of arsenic during ignition, in consequence of the reducing action of ammonia evolved in the process.t Another possible source of error is the solubility of ammonium magnesium arsenate in ammoniacal water and solutions of ammonium salts.I There is also the possibility that the constitution of ammonium magnesium arsenate as precipitated may not be ideal, in consequence of the action of ammonium salts known to be influential in determining the constitution of the analogous ammonium phosphates of magnesium and other elements. . Ann. Chim., 3, xvii, 501. t Wach and Rose, Schweigger, Jour. Ch. Phys., lix, 297. Reichel, Ann. Phys., Ixxvi, 20. Rammelsberg, Ber. Dtsch. chem. Ges., xiv, 279. Kaiser, Zeit. anal. Chem., xiv, 250. t Rose, Zeit. anal. Chem., ii...


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Product Details
  • ISBN-13: 9781235906060
  • Publisher: Rarebooksclub.com
  • Publisher Imprint: Rarebooksclub.com
  • Height: 246 mm
  • No of Pages: 164
  • Spine Width: 9 mm
  • Width: 189 mm
  • ISBN-10: 123590606X
  • Publisher Date: 01 May 2012
  • Binding: Paperback
  • Language: English
  • Returnable: N
  • Weight: 304 gr


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