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Modern Coking Practice; Including the Analysis of Materials and Products: A Handbook for Those Engaged in Coke Manufacture and the Recovery of Bye-Pro

Modern Coking Practice; Including the Analysis of Materials and Products: A Handbook for Those Engaged in Coke Manufacture and the Recovery of Bye-Pro


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About the Book

This historic book may have numerous typos and missing text. Purchasers can usually download a free scanned copy of the original book (without typos) from the publisher. Not indexed. Not illustrated. 1910 edition. Excerpt: ...and its contents rinsed into a porcelain basin and titrated with a normal solution of soda, 6-35 c.c. being required to neutralise the remaining acid. Hence the acid neutralised by the ammonia liberated from-25 gram of the salt = 100-6-35 = 365 c.c., and 3-65 x-017 = '062 gram NH3. That is, -25 gram contains-062 c c. 1-00 -248, or 100 contain 24-8 c.c. That is, 24-8 per cent. ammonia in the salt. The amount of moisture in sulphate may be determined by weighing off 5 or 10 grams, and drying in a water bath at a temperature of 100 Cent. for about two hours until the weight becomes constant. The loss represents moisture. The free acid present is determined by dissolving 5 grams of the salt in distilled water, adding a few drops of methyl orange solution and titrating with standard soda. If great accuracy is necessary, it is advisable to use decinormal soda, that is, one-tenth the strength of the normal, or-004 gram hydrate per 1 c.c. The Formation of Blue Salt.--As previously mentioned, the occurrence of blue salt is not uncommon under certain working conditions, and much time and thought have been spent in endeavouring to prevent its formation, more particularly because the colour affects the marketable value. The cause of the blue colour was not very difficult to diagnose. It evidently arose from the presence of a ferrous salt and a ferrocyanide in the saturator liquor. The presence of the iron salt could be accounted for in several ways. For instance, it might be originally present in the sulphuric acid used to absorb the ammonia, or the acid might have come in contact with iron or steel in some part of the plant, but the presence of ferrocyanide was not so easy to explain. For those who are interested sufficiently in the matter, ...


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Product Details
  • ISBN-13: 9781234949075
  • Publisher: Rarebooksclub.com
  • Publisher Imprint: Rarebooksclub.com
  • Height: 246 mm
  • No of Pages: 52
  • Spine Width: 3 mm
  • Weight: 109 gr
  • ISBN-10: 1234949075
  • Publisher Date: 01 Oct 2012
  • Binding: Paperback
  • Language: English
  • Returnable: N
  • Sub Title: A Handbook for Those Engaged in Coke Manufacture and the Recovery of Bye-Pro
  • Width: 189 mm


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