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Graphite; Its Properties, Occurrence, Refining and Uses

Graphite; Its Properties, Occurrence, Refining and Uses


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About the Book

This historic book may have numerous typos and missing text. Purchasers can usually download a free scanned copy of the original book (without typos) from the publisher. Not indexed. Not illustrated. 1907 edition. Excerpt: ...to go into solution. The hydrochloric acid dissolves the liberated metal oxides, but the method cannot give accurate results, because one is never sure whether the final residue is really pure carbon. Of the methods proposed for rapid determination of carbon in graphite, that of Gintlf may be described. Gintl uses a stout tube of refractory glass 10 to 12 centimeters long and about 1 centimeter wide, sealed at one end and blown out to a small sized bulb. He brings into this tube 0.05 to 0.1 gram of the graphite, dried at 150 to 180, and added to this 1.5 to 3 grams of pure pulverized Dinglers Polyt. Journal, 137-445. t Ibid. lead oxide, previously ignited. The whole is then weighed and the lead oxide with the graphite thoroughly mixed by means of a mixing wire; that part of the tube, in which the charge has been placed, is then heated at first over a Bunsen burner, and finally with a blow pipe lamp, until the contents are completely fused and froth is no longer noticeable. According to Gintl this operation is completed in ten minutes. The whole is then allowed to cool, and from the loss in weight, which represents the carbon dioxide, calculate the carbon. Of course, the results obtained by this method are serviceable only when the graphite contains neither water chemically combined or capable of expulsion at 150 to 180 C., nor carbonates, and when all the carbon is oxidized by fusion with the lead oxide. G. C. Wittstein recommends also the well known method of Berthier, used for the determination of the pyrometric value of a substance. One gram of finely powdered graphite is mixed with 25 grams of pulverized oxide of lead, the charge is placed in an unglazed porcelain crucible and then covered with 25 grams of oxide of lead; the whole is...


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Product Details
  • ISBN-13: 9781234888039
  • Publisher: Rarebooksclub.com
  • Publisher Imprint: Rarebooksclub.com
  • Height: 246 mm
  • No of Pages: 90
  • Spine Width: 5 mm
  • Width: 189 mm
  • ISBN-10: 1234888033
  • Publisher Date: 12 Oct 2012
  • Binding: Paperback
  • Language: English
  • Returnable: N
  • Weight: 177 gr


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