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Separation of Certain Acidic Oxides with Selenium Oxychloride

Separation of Certain Acidic Oxides with Selenium Oxychloride


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This historic book may have numerous typos and missing text. Purchasers can usually download a free scanned copy of the original book (without typos) from the publisher. Not indexed. Not illustrated. 1921 edition. Excerpt: ... cc. SeOClg, when boiled for a few minutes or when digested in a sealed tube on a steam sand bath for E4 hours, was therefore adopted as a somewhat arbitrary criterion, by which a given specimen of MoO3 could be adjudged to be "soluble" or "insoluble." Three possible explanations suggest themselves for the relatively greater solubility of hydrated MoO3. In the first place, the effect may be due to hydrolysis of the solvent by the water present in the oxide. If this were true, the addition of small amounts of water to the solution should cause ignited MoO3 to become soluble to the same extent as the hydrated form. Experiments showed that this is not the case. It may be mentioned at this point that it is very difficult to wash the precipitated, hydrous MoO3 free from ammonia and other substances which are adsorbed very tenaciously by the precipitate. The addition of ammonium salts and other possible impurities, such as HgSO and HNO3, in quantities corresponding to those found byanalysis in the precipitate, has no effect upon the solubility of the ignited oxide in SeOClg. In the second place, the solubility may be due to the existence of a definite hydrate, soluble in SeOClg. If this were true, the solubility of the oxide should vary with the water content. So long as the water content exceeded that of the soluble hydrate, gradual removal of the water should not effect the solubility. Whem, however, the percentage of water was reduced below that necessary to form the soluble hydrate, a mixture of this compound and the anhydride (or a lower, insoluble hydrate), would be produced, and the sample would cease to be completely soluble in SeOClg. The amount remaining undissolved would increase regularly with further removal of...


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Product Details
  • ISBN-13: 9781234367770
  • Publisher: Rarebooksclub.com
  • Publisher Imprint: Rarebooksclub.com
  • Height: 246 mm
  • No of Pages: 24
  • Spine Width: 1 mm
  • Width: 189 mm
  • ISBN-10: 1234367777
  • Publisher Date: 22 Jan 2013
  • Binding: Paperback
  • Language: English
  • Returnable: N
  • Weight: 64 gr


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