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Quantitative Chemical Analysis Volume 2

Quantitative Chemical Analysis Volume 2


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About the Book

This historic book may have numerous typos and missing text. Purchasers can usually download a free scanned copy of the original book (without typos) from the publisher. Not indexed. Not illustrated. 1908 edition. Excerpt: ...capacious flask, adding nitric acid gradually until the carbon dioxide and nitric-oxide gas evolved by the decomposition of the excess of sulphocyanic acid ceases; then evaporate nearly to dryness, dilute, filter if necessary, neutralize the free acid in a flask (to avoid loss from spirting), heat the almost neutral liquid until the carbon dioxide is expelled, transfer the liquid to a porcelain dish, and precipitate the zinc with sodium carbonate according to Vol I, p. 287, 1, a. Make certain, on the one hand, that the filtrate contains no weighable quantities of zinc, by testing with ammonium sulphide; and, on the other hand, test the weighed zinc oxide as to its purity. For this purpose boil it repeatedly with water, filter into a platinum dish, evaporate to dryness, gently ignite the slight residue of alkali salts, and deduct its weight from that of the zinc oxide, provided it is completely soluble in water, otherwise it must be filtered and the clear solution again evaporated. Then ascertain if the zinc oxide is completely soluble in hydrochloric acid, and if necessary determine any residual silicic acid, and deduct its weight also from that of the zinc oxide; finally supersaturate the cold zinc-chloride solution, after diluting it, with ammonia, in order to ascertain whether any weighable trace of ferric oxide remains undissolved. If necessary, this is collected, washed, again dissolved in hydrochloric acid, and the solution reprecipitated with ammonia in order to obtain the ferric hydroxide free from zinc. Instead of determining the zinc in the manner above detailed it may be determined by Zimmermann's method, precipitating as zinc sulphide and weighing as such (see p. 661, First Method). Second Method. 2. Proceed just as in the...


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Product Details
  • ISBN-13: 9781234109554
  • Publisher: Rarebooksclub.com
  • Publisher Imprint: Rarebooksclub.com
  • Height: 246 mm
  • No of Pages: 450
  • Spine Width: 23 mm
  • Width: 189 mm
  • ISBN-10: 1234109557
  • Publisher Date: 14 Jan 2013
  • Binding: Paperback
  • Language: English
  • Returnable: N
  • Weight: 798 gr


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