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Circular Volume 859-865

Circular Volume 859-865


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This historic book may have numerous typos and missing text. Purchasers can download a free scanned copy of the original book (without typos) from the publisher. Not indexed. Not illustrated. Excerpt: ...over activated copper, then elution-column chromatography (gravimetrics) on silica gel. The saturated paraffinnaphthene fractions were analyzed both qualitatively and quantitatively on Perkin-Elmer Sigma 2-B and 3920 gas chromatographs, respectively. Both systems were supported by Sigma 10 data microprocessors. The qualitative gas chromatographic analyses were performed on 8 ft X 0.125 in. (2.4 m X 0.318 cm) stainless steel columns packed with 3 percent OV-101, 100-to 200-mesh (150-to 75-/im) GCQ. The column temperature was 176 F (80 C) at injection and was programmed to increase initially at a rate of 29 F/min (16 Citron) for 8 minutes and then at a rate of 14 F/min (8 C/min) to a final temperature of 572 F (300 C). Quantitative analyses were performed on an OV-1 50-ft (15-m) SCOT column. The column was held for one minute at an injection temperature of 212 F (100 C); it was then programmed to increase at 7 F/min (4 C/min) to a final temperature of 473 F (245 C) and held at the final temperature until n-Cjj eluted. The following expression, modified from Hunt (1974), was used to calculate the Carbon Preference Index (CPI): Total organic carbon is a measure of the organic richness of a source rock. Triplicate total organic carbon analyses were performed by the USGS on dried, weighed aliquots of the carbonate-free residue produced by leaching with hot, 6-normal hydrochloric acid of approximately 0.07 oz avdp (0.2 g) of ground sample smaller than 60 mesh (250 /im). The samples were combusted in a Perkin-Elmer model 240 Carbon, Hydrogen, Nitrogen Analyzer. The organic carbon analyses for the thermal pyrolysis studies were performed by Rhinehart Laboratories, Arvada, Colo., on sample aliquots using the chromic oxidation method outlined by Bush (1970). The thermal py...


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Product Details
  • ISBN-13: 9781231194515
  • Publisher: Rarebooksclub.com
  • Publisher Imprint: Rarebooksclub.com
  • Height: 246 mm
  • No of Pages: 178
  • Spine Width: 10 mm
  • Width: 189 mm
  • ISBN-10: 1231194510
  • Publisher Date: 01 May 2012
  • Binding: Paperback
  • Language: English
  • Returnable: N
  • Weight: 327 gr


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