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I.C.S. Reference Library Volume 81

I.C.S. Reference Library Volume 81


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This historic book may have numerous typos and missing text. Purchasers can download a free scanned copy of the original book (without typos) from the publisher. Not indexed. Not illustrated. 1905 Excerpt: ...and the beaker nearly filled up with cold water. It is allowed to settle, and the clear liquid poured off for use. This starch solution should be made up fresh every time, as it will not keep more than a day. 13. Determination of Sulphur Dioxide.--The apparatus used in this determination is known as Reich's apparatus; it consists of a double-necked absorption bottle a, the aspirator b, and the glass cylinder e. These are supported by a convenient stand, as shown in Fig. 3. The rubber tube joining a and b is about 30 centimeters long; 71 100 cubic centimeters of the iodine solution are placed in the bottle a, and the aspirator b is filled with water. Before making a determination, the air in the tubes leading to the apparatus is displaced by the gas to be examined. The apparatus is tight if, after a short time and as soon as the air in a is correspondingly expanded, the water ceases entirely to flow from the aspirator. In making the determination, the stop-cock c is opened, and the amount of water that is necessary to draw over sufficient gas to decolorize the iodine solution is measured in the cylinder e. During the determination, the bottle a is frequently shaken. The volume of water that has run out is equal to that of the gas taken, FK5-8 and the quantity of sulphur dioxide can approximately be told from the amount of iodine used. During the experiment, the temperature of the water is taken (which will be the temperature of the gas) and the height of the barometer is noted. When 8 or 10 liters of gas have in this way been aspirated through the iodine solution, the process is stopped, and 25 cubic centimeters of the iodine solution are transferred to a beaker and titrated with the standard sodium thiosulphate. As soon as the red-brown color of the iodine ...


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Product Details
  • ISBN-13: 9781231094679
  • Publisher: Rarebooksclub.com
  • Publisher Imprint: Rarebooksclub.com
  • Height: 246 mm
  • No of Pages: 132
  • Spine Width: 7 mm
  • Width: 189 mm
  • ISBN-10: 1231094672
  • Publisher Date: 01 May 2012
  • Binding: Paperback
  • Language: English
  • Returnable: N
  • Weight: 249 gr


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