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The Analysis of Permissible Explosives Volume 96-103

The Analysis of Permissible Explosives Volume 96-103


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About the Book

This historic book may have numerous typos and missing text. Purchasers can download a free scanned copy of the original book (without typos) from the publisher. Not indexed. Not illustrated. 1916 Excerpt: ...the nitroglycerin determined by difference. The direct Storm, C. G., Effect of nltrotoluenes on the determination of nitroglycerin by means of the nitrometer: Original Communications; 8th Int. Cong. App. Chem., vol. 4, 1912, p. 117. '" determination of these ether-soluble materials is discussed in pages 46 and 47. TESTS TO ASCEKTAIN SOLUBILITY OF ETHER-SOLUBLE SUBSTANCES IN NITROGLYCERIN. A series of tests was made to ascertain the extent to which the solubility of these ether-soluble substances in the nitroglycerin would affect the determination of the purity of the nitroglycerin separated from such substances by filtration. About 0.5 gram of the substance taken for test was added to 2 c. c. of nitroglycerin of known nitrogen content (18.42 per cent), the whole dissolved in 50 c. c. of ether, the ether evaporated by the method described for treating the ether extract of an explosive (pp. 35 and 36), the evaporated material filtered through a paper filter, and the clear filtrate tested in the nitrometer. From the result of the nitrogen determination it is readily ascertained whether an appreciable quantity of the substance has been dissolved by the nitroglycerin. For example, a determination giving a nitrogen content of 18.32 per cent indicates that 1 per cent of the substance is dissolved in the filtered nitroglycerin; 18.13 per cent N indicates that 2 per cent of the substance has been dissolved, and so on, provided that any nitrogen taken up by the dissolved materia is disregarded. The table following shows the results of the tests made: Results of tests to determine nitrogen content in nitroglycerin filtered from various ether-soluble substances. o Melting point, 66 to 68 C & Melting point, 81 to 82 C. The above results show that vaseline, para...


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Product Details
  • ISBN-13: 9781155018324
  • Publisher: Rarebooksclub.com
  • Publisher Imprint: Rarebooksclub.com
  • Height: 246 mm
  • No of Pages: 34
  • Spine Width: 2 mm
  • Width: 189 mm
  • ISBN-10: 115501832X
  • Publisher Date: 01 May 2012
  • Binding: Paperback
  • Language: English
  • Returnable: N
  • Weight: 82 gr


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