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The Testing and Valuation of Raw Materials Used in Paint and Colour Manufacture

The Testing and Valuation of Raw Materials Used in Paint and Colour Manufacture


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This historic book may have numerous typos and missing text. Purchasers can download a free scanned copy of the original book (without typos) from the publisher. Not indexed. Not illustrated. 1900. Excerpt: ... amount of Fe203 + A1203. To estimate the amount of calcium salts present, the filtrate mentioned above is raised to the boil, a little more ammonium hydrate is added, and a few cc. of a saturated solution of ammonium oxalate. The whole is well boiled for ten minutes, and if any calcium salt is present, it will be indicated by a white precipitate. This is carefully filtered on to a Swedish filter-paper, the precipitate being well washed on the filter, and the whole then placed in an air-bath to dry. When this is accomplished, the precipitate is ignited in a platinum crucible, the filterpaper being ignited before the bulk of the precipitate is added, and the whole is heated over the blowpipe for fifteen minutes. The result after deducting the weight of the crucible and ash will give the amount of calcium salt as oxide, contained in the original sample, and from this it will be necessary to calculate the oxide into sulphate, as it was doubtless present in that form in the sample, and in this connection it may be stated that 56 parts of CaO are equal to 172 parts of CaS04 + 2 H20 (gypsum). If the sample under examination is suspected to contain magnesium compounds, the filtrate from the last operation, which has been carefully preserved, is boiled down in a flask to reduce its bulk somewhat. It is then cooled, placed in a large beaker, and rendered alkaline by the addition of ammonium hydrate, after which about 50 cc. of a saturated solution of sodium phosphate are stirred in. The beaker is allowed to stand overnight, as the precipitate often takes a long time to form, and in the morning it is carefully filtered on to a Swedish filter-paper, the precipitate being then well washed with distilled water, to which has been added a little ammonium hydrate. The fil...


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Product Details
  • ISBN-13: 9781151595591
  • Publisher: General Books
  • Publisher Imprint: General Books
  • Height: 246 mm
  • No of Pages: 24
  • Spine Width: 1 mm
  • Width: 189 mm
  • ISBN-10: 1151595594
  • Publisher Date: 01 Feb 2012
  • Binding: Paperback
  • Language: English
  • Returnable: N
  • Weight: 64 gr


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