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Home > Art, Film & Photography > Handbook of Chemical Analysis for Practical Men; Containing Directions for Examining and Valuing Several Hundreds of the Most Important Articles of Commerce, Manufacturing Products, Residues, Etc. Also, a Brief Systematic Course of Quantitative Ana
Handbook of Chemical Analysis for Practical Men; Containing Directions for Examining and Valuing Several Hundreds of the Most Important Articles of Commerce, Manufacturing Products, Residues, Etc. Also, a Brief Systematic Course of Quantitative Ana

Handbook of Chemical Analysis for Practical Men; Containing Directions for Examining and Valuing Several Hundreds of the Most Important Articles of Commerce, Manufacturing Products, Residues, Etc. Also, a Brief Systematic Course of Quantitative Ana


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About the Book

This historic book may have numerous typos or missing text. Not indexed. Purchasers can download a free scanned copy of the original book (without typos) from the publisher. 1861. Not illustrated. Excerpt: ... 150. PHOSPHORUS IN IRON ORES AND METALLIC IRON. a. Dissolve in nitric acid, add hydrochloric acid, and evaporate to a sirupy consistence. The residue is diluted with water, and the solution poured, drop by drop, into a mixture of protosulphuret of potassium and silicate of potash. To 10 grains of iron should be employed 50 grains sulphuret of potassium, and 10 grains of a soluble glass prepared by fusing 1 part of powdered quartz with 2 parts of a mixture of 5 parts carbonate of potash and 4 parts carbonate of soda. The precipitate which is formed contains iron as sulphuret, and silicates of lime, magnesia, and alumina. To prevent any sulphuret from dissolving, an excess of recently-prepared carbonate of lead is added before filtration. The precipitate is thrown on a filter, and washed with water containing l-10th of its bulk of saturated solution of carbonate of ammonia and a little caustic ammonia. The filtered liquid is evaporated almost to dryness, and the residue moistened with hydrochloric acid to separate the silica. The solution contains all the phosphorus as phosphoric acid. Mix with tartaric acid, and determine the phosphoric acid by acetate of magnesia. b. Dissolve 120 grains of tartaric acid in a little water. Dissolve in another portion of water 210 grains of cyanide of potassium, so as to make a very strong solution. Meantime dissolve 15 grains of the sample of iron in nitric acid, to which a little hydrochloric has been added. The tartaric acid is then poured into the iron, some sulphate of magnesia is added, then a considerable excess of ammonia, and lastly the cyanide of potassium. A deep red liquid is thus obtained, and sulphuret of potassium is added, drop by drop, until the liquor which first becomes of a light yellow again...


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Product Details
  • ISBN-13: 9781150219429
  • Publisher: General Books
  • Publisher Imprint: General Books
  • Height: 246 mm
  • No of Pages: 92
  • Spine Width: 5 mm
  • Width: 189 mm
  • ISBN-10: 1150219424
  • Publisher Date: 01 Jan 2012
  • Binding: Paperback
  • Language: English
  • Returnable: N
  • Weight: 181 gr


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Handbook of Chemical Analysis for Practical Men; Containing Directions for Examining and Valuing Several Hundreds of the Most Important Articles of Commerce, Manufacturing Products, Residues, Etc. Also, a Brief Systematic Course of Quantitative Ana
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