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Methods for the Analysis of Ores, Pig Iron and Steel in Use at the Laboratories of Iron and Steel Works in the Region about Pittsburg, Pa

Methods for the Analysis of Ores, Pig Iron and Steel in Use at the Laboratories of Iron and Steel Works in the Region about Pittsburg, Pa


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About the Book

This historic book may have numerous typos and missing text. Purchasers can download a free scanned copy of the original book (without typos) from the publisher. Not indexed. Not illustrated.1898 Excerpt: ... NOTES ON THE ANALYSIS OF MILL AND PUDDLE CINDERS. By Jos. M. W1lson. Mill cinder is used in our furnace as part of the burden and is almost wholly brought in car-load lots. As the railroad people are constantly pushing us for prompt unloading, methods for rapid determination of the constituent elements of these cinders are important, Formerly we were required to report the iron and insoluble matter at once and later the silica. At present iron and phosphorus are also required and occasionally manganese. Our methods are as follows: IRON. Weigh out 0.25 and 0.5 gram into lipless beakers, moisten with 10-15 cc. water, making certain that the mass is well broken up, add quickly 20 cc. concentrated hydrochloric acid, cover, boil gently for twenty minutes (or let digest upon a steam-table one hour, then bring to a good boil), add stannous chloride solution, from a pipette, till the liquid is colorless, boil two minutes, remove to the steam-table and allow to settle. The supernatant liquid must be colorless. The residue will vary from light gray to black according to the amount of powdered coke present, Wash into a No. 5 or 6 beaker, rinse a small beaker thoroughly with cold water, taking care to remove all the insoluble matter. Make the volume 300 cc., stir well, add 30-40 cc. mercuric chloride solution, all at once, stir, run in potassium dichromate until 4 drops give no blue coloration with a drop of ferricyanide indicator in one-half minute. Solutions Used.--Potassium dichromate, 4.9 grams of the salt in 1 liter of water. 1 cc. = 0.005 gram iron. Stannous chloride, 100 grams in 1 liter hydrochloric acid (1: 1). Mercuric chloride, 50 grams in 1 liter of water. Ferricyanide indicator, 5 cc. of a 5 per cent, solution in 40 cc. water. INSOLUBLE MATTER AND SILICA. ...


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Product Details
  • ISBN-13: 9781150114175
  • Publisher: General Books
  • Publisher Imprint: General Books
  • Height: 246 mm
  • No of Pages: 42
  • Spine Width: 2 mm
  • Width: 189 mm
  • ISBN-10: 1150114177
  • Publisher Date: 09 Feb 2012
  • Binding: Paperback
  • Language: English
  • Returnable: N
  • Weight: 95 gr


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