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Encyclopaedia of Chemistry, Theoretical Practical and Analytical, as Applied to the Arts

Encyclopaedia of Chemistry, Theoretical Practical and Analytical, as Applied to the Arts


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About the Book

This historic book may have numerous typos and missing text. Purchasers can download a free scanned copy of the original book (without typos) from the publisher. Not indexed. Not illustrated. 1879 Excerpt: ... of potash and acidified, destroys its magnificent red tint, at the same time effervescing from the escape of carbonic acid; and when the solid body, mixed with black oxide of manganese, is treated with diluted sulphuric acid, an effervescence of the same gas will also be noticed. Estimation.--1. As Carbonate of Lime.--The solution, freed, if necessary, from carbonates by boiling with a slight excess of hydrochloric acid, is either neutralized or rendered slightly acid with acetic acid by adding sodium acetate. A sufficiency of acetate of lime is then added, and the fine precipitate of oxalate of lime allowed to subside. The supernatant fluid is decanted through a filter, and the precipitate washed on to it with hot water, taking care to allow each portion to pass completely through before adding more. After washing completely, the precipitate is ignited in a platinum crucible to bare redness, the filter ash added, and the carbonate of lime, resulting from decomposition of the oxalate, weighed. If too strongly ignited, the residue will show a strong alkaline reaction when moistened and placed upon litmus paper. It must be washed into the crucible, moistened with carbonate of ammonia solution, again gently ignited, and re-weighed. One part of carbonate of lime corresponds to 126 part of crystallized oxalic acid, or-88 part of C204. The solution must not contain magnesium salts in quantity, or manganese, iron, chromium, aluminium, copper, or any heavy metal. ( Vide Oxalate of Lime, ante). 2. As Oxalate of Lime.--The solution must be precipitated, &c, as above directed; but collected upon a weighed filter, which is then dried and heated on the water bath till its weight is constant The gain in weight of the filter will give the amount of CaC2O4.H20, each p...


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Product Details
  • ISBN-13: 9781130404395
  • Publisher: Rarebooksclub.com
  • Publisher Imprint: Rarebooksclub.com
  • Height: 246 mm
  • No of Pages: 840
  • Spine Width: 42 mm
  • Width: 189 mm
  • ISBN-10: 1130404390
  • Publisher Date: 01 Mar 2012
  • Binding: Paperback
  • Language: English
  • Returnable: N
  • Weight: 1470 gr


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