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Elements of Chemical Analysis; Qualitative and Quantitative

Elements of Chemical Analysis; Qualitative and Quantitative


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This historic book may have numerous typos and missing text. Purchasers can download a free scanned copy of the original book (without typos) from the publisher. Not indexed. Not illustrated. 1845 Excerpt: ...carbonate of barytes on the filter, and determining the number of measures of test acid necessary for the neutralization of the filtered liquid. That number represents the amount of caustic alkali present in grains. SECTION III. AMMONIA. If the ammonia whose amount is to be estimated exists in aqueous solution, and in the free state unaccompanied by ammoniacal salts except the muriate, a slight excess of hydrochloric acid is added, and the solution is evaporated to dryness in a weighed platinum capsule, by means of a waterbath. When dry, the residue is weighed, again heated in the water-bath and weighed. This is repeated so long as it suffers any loss. From the weight of the muriate of ammonia obtained, that of the ammonia is calculated: 1 part of muriate of ammonia represents 0-32077 of absolute ammonia. After the last weighing, the capsule is heated strongly, to sublime the muriate of ammonia. The loss now experienced, which should be pure muriate of ammonia, affords another datum in the calculation. This method of estimating ammonia is not strictly exact, inasmuch as a minute quantity of muriate of ammonia volatilizes during the evaporation to dryness; but the quantity lost is so very small as not to be appreciated without an extremely delicate balance. The following, however, is a more precise method. To the ammoniacal liquid, slightly supersaturated with hydrochloric acid, a solution of chloride of platinum is added, and the mixture is evaporated to dryness. The dry residue is digested in a mixture of two measures of alcohol, and one measure of ether, in which liquid the excess of chloride of platinum dissolves, and leaves the double chloride of platinum and ammonium undissolved. If the liquid has a yellow colour, sufficient chloride of platinum has be...


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Product Details
  • ISBN-13: 9781130363944
  • Publisher: Rarebooksclub.com
  • Publisher Imprint: Rarebooksclub.com
  • Height: 246 mm
  • No of Pages: 170
  • Spine Width: 9 mm
  • Width: 189 mm
  • ISBN-10: 1130363945
  • Publisher Date: 01 Mar 2012
  • Binding: Paperback
  • Language: English
  • Returnable: N
  • Weight: 313 gr

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