A Systematic Handbook of Volumetric Anaylsis - Bookswagon UAE
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A Systematic Handbook of Volumetric Anaylsis

A Systematic Handbook of Volumetric Anaylsis


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This historic book may have numerous typos and missing text. Purchasers can download a free scanned copy of the original book (without typos) from the publisher. Not indexed. Not illustrated. 1904 Excerpt: ...gasometrically with permanganate, but 5 volumes of the O comes from the permanganate itself, and therefore such a solution is really only 5 volume. A true 10 volume solution should yield from itself, when fully decomposed, ten times its volume of O, and contain by weight 3-04 per cent, of H2O2 or 143 per cent, by weight of O. Kingzett (J. C. 5. 1880, 792) has shown that the best estimation of the hydrogen peroxide, contained in any given solution of it, is made by iodine and thiosulphate in the presence of a tolerably large excess of sulphuric acid, the reaction being--2HI + H202=2HilO + I.2. The function performed by the sulphuric acid is difficult of explanation, but the want of uniformity in the reaction experienced by many operators no doubt has arisen from the use of insufficient acid. Mbthod Of Procedure: This is done by mixing 10 c.c. of the peroxide solution to be examined with about 30 c.c. of dilute sulphuric acid (1: 2) in a beaker, adding crystals of potassium iodide in sufficient quantity, and after standing five minutes titrating the liberated iodine with N/io thiosulphate and starch. The peroxide solution should not exceed the strength of 2 volumes; if stronger, it must be diluted proportionately before the titration. In the case of a very weak solution it will be advisable to titrate with N/ioo thiosulphate. 1 c.c. N/io thiosulphate = 0 00085 gm. H, O2 or 0 0008 gm. O. A method of estimating the oxygen in hydrogen peroxide by permanganate was inserted in a previous edition of this book, but experience has proved it to be useless. Carpenter and Nicholson (Analyst ix. 36) report a series of experiments on the analysis of hydrogen peroxide, both by the iodine and permanganate methods. The conclusion they arrive at is, that the process of Kingzet..


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Product Details
  • ISBN-13: 9781130241396
  • Publisher: Rarebooksclub.com
  • Publisher Imprint: Rarebooksclub.com
  • Height: 246 mm
  • No of Pages: 300
  • Spine Width: 16 mm
  • Width: 189 mm
  • ISBN-10: 1130241394
  • Publisher Date: 01 Mar 2012
  • Binding: Paperback
  • Language: English
  • Returnable: N
  • Weight: 540 gr


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