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Analytical Chemistry for Technicians, Second Edition

Analytical Chemistry for Technicians, Second Edition


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About the Book

This book provides the practical skills needed to function as a competent technician in an analytical chemistry laboratory. It presents both theory together with "real-life" practical aspects. Building on the success of its predecessor, this stand-alone reference and training text has been fully revised and restructured to present a fresh and challenging approach.

Table of Contents:
INTRODUCTION TO CHEMICAL ANALYSIS Chemical Analysis Qualitative vs. Quantitative, Wet vs. Instrumental General Laboratory Considerations The Laboratory Notebook Gravimetric Analysis Analytical Calculations The Need for Stoichiometry Gravimetric Factors SAMPLING AND SAMPLE PREPARATIONS The Total Analysis Step One: Obtaining the Sample Step Two: Handling the Sample Step Three: Preparing the Sample for Analysis Quality Assurance of Reagents STATISTICS IN CHEMICAL ANALYSIS Terminology Distribution of Random Errors Rejection of Data - The Q Test Student's t Test Statistics in Quality Control CHEMICAL EQUILIBRIUM Review of Basic Concepts The Solubility of Precipitates The Solubility Product Constant Solubility and Ksp Addition of Ions from an External Source Chemical Equilibrium and Weak Acids Weak Bases Buffer Solutions INTRODUCTION TO TITRIMETRIC ANALYSIS Titration Defined Preparation of Molar Solutions Preparation from Pure Solid Chemicals Preparation by Dilution Volumetric Glassware Solution Standardization and Terminology When to be Accurate and When Not - Revisited Experiments ACID-BASE TITRATIONS AND CALCULATIONS Standardization Calculations Equivalents, Equivalent Means, and Normality Examples of Acid-Base Primary Standards and Calculations Percent Constituent Calculations Back Titrations The Kjeldahl Titration Millimoles and Milliequivalents Introduction to Titration Curves The Role of Indicators COMPLEXOMETRIC TITRATIONS AND CALCULATIONS Complex Ion Terminology The EDTA Ligand The Determination of Water Hardness Parts per Million Standardization and Calculations OXIDATION-REDUCTION AND OTHER TITRATIONS Oxidation Number Oxidation-Reduction Terminology The Ion Electron Method for Balancing Equations Equivalent Weights in Redox Reactions Potassium Permanganate Iodometry - An Indirect Method Summary of Redox Applications Non-Redox Precipitation Titrations ANALYSIS WITH INSTRUMENTS AND COMPUTERS Instrumental Data and Readout Methods for Quantitative Analysis Blanks and Controls Effects of Sample Pretreatment on Calculations Use of Computers Modern Data Handling FUNDAMENTALS OF LIGHT AND LIGHT ABSORPTION Nature and Parameters of Light Converting and Calculating Light Parameters Light Absorption and Emission Atomic vs. Molecular Names of Techniques and Instruments UV-VIS SPECTROPHOTOMETRY Instrument Design Qualitative and Quantitative Analysis The Question of Matched Cuvettes The Absorption Spectrum and lMAX Fluorometry INFRARED SPECTROMETRY Liquid Sampling Solid Samplilng Instrument Design Qualitative and Quantitative Analysis NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY AND MASS SPECTROMETRY Nuclear Magnetic Resonance Spectroscopy Mass Spectrometry ATOMIC SPECTROSCOPY Atomization and Excitation Flame Emission Flame Atomic Absorption Graphite Furnace Atomic Absorption Vapor Generation Methods Inductively Coupled Plasma Other Atomic Emission Techniques Summary of Atomic Techniques ANALYTICAL SEPARATIONS Recrystallization Distillation Liquid-Liquid Extraction Liquid-Solid Extraction Chromatography Electrophoresis GAS CHROMATOGRAPHY Instrument Design Sample Injection Columns Other Variable Parameters The Chromatogram Detectors Qualitative Analysis Quantitative Analysis Troubleshooting HIGH PERFORMANCE LIQUID CHROMATOGRAPHY Solvent Delivery Sample Injection Column Selection The Chromatogram Detectors Qualitative and Quantitative Analysis Troubleshooting ELECTROANALYTICAL METHODS Transfer of Electrons via Electrodes Transfer Tendencies - Standard Reduction Potentials Determination of Overall Redox Reaction Tendency: E0cell The Nernst Equation Potentiometry Polarography and Voltammetry APPLICATIONS SUMMARY Wet Methods Instrumental Methods Reference Sources Introduction to Automation APPENDICES Significant Figures Table of Some Ksp Values Table of Ka and Kb Values Compositions of Some Concentrated Commercial Acids and Bases Summary of Calculations for Titrimetric Analysis Recipes for Selected Acid-Base Indicator Solutions Basic Electrical Terminology Common Metric Prefixes Answers to Selected Questions and Problems Reference Sources **Each chapter includes an Introduction, as well as end-of-chapter Experiments and a Questions and Problems Section**

About the Author :
Kenkel; John Southeast Community College, Lincoln, Nebraska, USA,


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Product Details
  • ISBN-13: 9780873719667
  • Publisher: Taylor & Francis Inc
  • Publisher Imprint: CRC Press Inc
  • Edition: New edition
  • Language: English
  • No of Pages: 576
  • Weight: 1320 gr
  • ISBN-10: 0873719662
  • Publisher Date: 22 Jul 1994
  • Binding: Hardback
  • Height: 279 mm
  • No of Pages: 576
  • Returnable: N
  • Width: 216 mm


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