Cyclic Voltammetry
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Home > Mathematics and Science Textbooks > Chemistry > Analytical chemistry > Cyclic Voltammetry: Simulation and Analysis of Reaction Mechanisms
Cyclic Voltammetry: Simulation and Analysis of Reaction Mechanisms

Cyclic Voltammetry: Simulation and Analysis of Reaction Mechanisms


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About the Book

Cyclic Voltammetry is the only book solely devoted to its subject and containing a data analysis project written by the author. Beginning with the fundamentals of cyclic voltammetry from both an experimental and theoretical point of view, the author focuses on the applications in data interpretation with emphasis on chemical reactions and electrode reduction potentials. The PC compatible computer program that accompanies the book provides the experimentalists with a simulation-based approach for the analysis of cyclic voltammograms. A survey format is utilized to discuss the use of CV for the study of reaction mechanisms in diverse branches of chemistry. The author then presents the method of simulation by explicit finite differences, the most commonly employed numerical method of CV analysis. The CVSIM program, written by the author and used in several countries, simulates cyclic voltammetric experiments. It is explained along with DSTEP, a general program for the simulation of double potential step experiments. Next the author describes CVFIT to find the least squares best fit between experimental and simulated cyclic voltammograms. Chemists of all types as well as academic and industrial researchers and graduate level students are certain to find cyclic voltammetry a useful, valuable and long overdue addition to the field.

Table of Contents:
Useful Equations; 1. The Reduction Potential and Electrode Kinetics; 1.1 The Reduction Potential; 1.2 Electrode Kinetics; References; 2. The Cyclic Voltammetric Experiment; 2.1 An Overview; 2.2 The Electrochemical Cell; 2.3 Electrochemical Mechanisms: E&C Notation; 2.4 Distortions of the Faradaic Response; 2.5 Microelectrodes and Fast Scan Voltammetry; 2.6 Potential Step Methods and Cyclic Voltammetry; 2.7 Construction of a Fast Potentiostat; 2.8 Determination of the Number of Electrons; References; 3. A Survey of Electrochemical Mechanisms; 3.1 The CE Mechanism; 3.2 Multielectron Transfer; 3.3 Protonations at Equilibrium; 3.4 Catalytic Mechanisms; 3.5 The Reduction of Nitrobenzoic Acid; 3.6 Reduction of the Nit rosonium Cation and Its Complexes; 3.7 Reactivity of 17--, 18--, and 19--Electron Tungsten Complexes; 3.8 Mechanisms Involving Adsorption; References; 4. The Simulation of Electrochemical Experiments; 4.1 The Discretized Diffusion Equation; 4.2 Evaluation of the Boundary Conditions; 4.3 Dimensionless Units; 4.4 Solution Chemical Kinetics; 4.5 A Sample Simulation Program; References; 5. CVSIM: A General Program for the Simulation of Cyclic Voltammetry Experiments; 5.1 An Overview of CVSIM; 5.2 Extensions of the Simulation Method; 5.3 Accuracy of Simulations; 5.4 Installation and Use of CVSIM and CVGRAF; 5.5 Examples; References; 6. CVFIT: Simplex Data Analysis with CVSIM; 6.1 CVFIT: Simplex Data Analysis with CVSIM; 6.2 Instructions for the use of CVFIT; 6.3 A Prototype Analysis: The EC Mechanism; 6.4 Some Final Comments on Simulation Analysis; References; Appendix: Summary of Instructions for CVSIM, CVGRAF, CVFIT, and DSTEP; Index


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Product Details
  • ISBN-13: 9780471188032
  • Publisher: John Wiley and Sons Ltd
  • Publisher Imprint: John Wiley & Sons Inc
  • Height: 236 mm
  • Returnable: N
  • Weight: 369 gr
  • ISBN-10: 0471188034
  • Publisher Date: 20 Sep 1993
  • Binding: Hardback
  • Language: English
  • Sub Title: Simulation and Analysis of Reaction Mechanisms
  • Width: 154 mm


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