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Select Methods in Chemical Analysis (Chiefly Inorganic)

Select Methods in Chemical Analysis (Chiefly Inorganic)


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Purchase of this book includes free trial access to www.million-books.com where you can read more than a million books for free. This is an OCR edition with typos. Excerpt from book: ferric salt reduced by zinc or other reducing agent, and titrated volumetrically by permanganate or otherwise. (/) When the lead sulphate is to be determined, it may be done by treating a considerable quantity, say 20 grammes, with water, and boiling the insoluble residue with strong hydrochloric acid till the lead sulphate is entirely dissolved; from this solution lead sulphide may be thrown down by sulphuretted hydrogen, and the lead determined in the ordinary way. (/) If magnesium sulphate is to be determined, it rnay be done by dissolving a known weight, say 20 grammes, in hydrochloric acid, adding ammonia and ammonium oxalate, precipitating the magnesium from the nitrate by a phosphate, and ultimately weighing the magnesium pyrophosphate. (h) If the preceding determinations have been carefully conducted, the difference between 100 and the sum of them may be safely taken as sodium sulphate; if this is to be directly determined, however, it may be done either by determining the total sulphuric acid present by dissolving a known weight of salt-cake in hydrochloric acid, precipitating by barium chloride, and weighing the barium sulphate; subtracting the sulphuric acid contained as calcium sulphate, sodium bisulphate, magnesium sulphate, and lead sulphate, the remainder being calculated as sodium bisulphate; or by adding ammonia and ammonium oxalate to the aqueous solution of a known weight, and estimating the residue left on evaporation of the filtrate and ignition with sulphuric acid; on subtraction from this of the amounts due to magnesium sulphate, sodium chloride, and sodium bisulphate, the sodium sulphate is directly ascertained. The total ' available sodium sulphate ' is known by adding TVff of the sodium bisulphate to the amount of sodium sulphate found. ...


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Product Details
  • ISBN-13: 9780217868013
  • Publisher: Rarebooksclub.com
  • Publisher Imprint: Rarebooksclub.com
  • Height: 246 mm
  • No of Pages: 340
  • Spine Width: 18 mm
  • Width: 189 mm
  • ISBN-10: 0217868010
  • Publisher Date: 01 May 2012
  • Binding: Paperback
  • Language: English
  • Returnable: N
  • Weight: 608 gr


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