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Analysis of Metallurgical and Engineering Materials; A Systematic Arrangement of Laboratory Methods

Analysis of Metallurgical and Engineering Materials; A Systematic Arrangement of Laboratory Methods


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This historic book may have numerous typos and missing text. Purchasers can download a free scanned copy of the original book (without typos) from the publisher. Not indexed. Not illustrated. 1912. Excerpt: ... Determination of Zinc 1. Reagents.--Pure Zinc Oxide; Ammonium Chloride Solution, one per cent.; Potassium Ferrocyanide Solution, containing 21.63 grams of potassium ferrocyanide and seven grams of sodium sulphite to the liter; Uranium Nitrate, Indicator, prepared by dissolving 10 grams in 100 cc. of a five per cent. acetic acid solution. 2. Standardization of the Potassium Ferrocyanide Solution.--Dissolve half a gram of pure, recently ignited zinc oxide in a No. 3 beaker with 20 cc. of hydrochloric acid (1:1); neutralize with ammonia, then add 10 cc. excess of strong hydrochloric acid, and dilute the solution for titration to about 180 cc. Heat the zinc solution to 60 deg. C., then run in the potassium ferrocyanide solution from a burette until the zinc is almost completely precipitated, then, after adding successively 0.2 cc. of the ferrocyanide, rinsing down the sides of the beaker and stirring, remove test drops on the stirring rod, and mix them with four drop portions of the indicator on a white, paraffined tile. The precipitate assumes three, distinct forms during the titration, giving the solution the appearance of skimmed milk, then separating in a flocculent form, and finally diffusing and remaining suspended for a time. The flocculent precipitate usually appears when about three cc. of ferrocyanide are required to complete the titration. A permanent brown tinge indicates the end point. The weight cf zinc in the zinc oxide taken, divided by the number of cc. of ferrocyanide required, gives the weight of zinc corresponding to one cc. 3. Determination.--Transfer one gram of the finely ground ore to a 250 cc. Erlenmeyer flask; add 15 cc. of a mixture of equal parts of strong nitric and hydrochloric acids; warm gently with occasional shaking until dec...


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Product Details
  • ISBN-13: 9780217776127
  • Publisher: General Books
  • Publisher Imprint: General Books
  • Height: 246 mm
  • No of Pages: 30
  • Spine Width: 2 mm
  • Width: 189 mm
  • ISBN-10: 0217776124
  • Publisher Date: 03 Feb 2012
  • Binding: Paperback
  • Language: English
  • Returnable: N
  • Weight: 73 gr


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