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An Outline of Qualitative Analysis

An Outline of Qualitative Analysis


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Purchase of this book includes free trial access to www.million-books.com where you can read more than a million books for free. This is an OCR edition with typos. Excerpt from book: H3P04 and H2C204 are present in a solution, CaS04 will precipitate both, but acetic acid will dissolve the calcium phosphate only, and in such a case H3P04 must be tested for as well as II2- Analysis Of Unknown Substances. In the examination of any substance the following course is carried out: 1. ? Reduce the solid to a powder and boil with about ten times its quantity of water. Should a residue remain, allow it to settle and decant or- clear by filtration. A small quantity of the clear nitrate is evaporated to dryness on a clean platinum foil, if a residue remains the solution is treated according to Scheme A, page 3fi. '2. ? The residue insoluble in water is transferred to a beaker HN03 poured over it and then gently heated to boiling. Note whether nitrogen oxides are evolved, indicating the oxidation of a metal or some other body. Note whether sulphur separates. If a residue remains, filter, and wash first with a little dilute acid and then with water. Evaporate the filtrate and washings to dryness in order to remove the excess of HN03 redissolve in hot water and treat according to Scheme A, page 36. 3. ? The portion insoluble in HN03 is now heated with hot aqua regia. The solution diluted and the insoluble residue filtered and washed with water. The filtrate and washings evaporated to dryness, and then redissolved in hot water acidulated with HCl if necessary, to keep the substance in solution. The analysis is then carried on according to Scheme A, page 36. 4. ? Should there still remain a portion insoluble in acids, it is likely to be either a sulphate (of barium, strontium or lead); a chloride, bromide or iodide of silver or lead; or a silicate; and must befused with a fixed alkaline carbonate when the constituents are transposed in such manner as to rend...


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Product Details
  • ISBN-13: 9780217173667
  • Publisher: Rarebooksclub.com
  • Publisher Imprint: Rarebooksclub.com
  • Height: 246 mm
  • No of Pages: 18
  • Spine Width: 1 mm
  • Width: 189 mm
  • ISBN-10: 0217173667
  • Publisher Date: 05 Jul 2012
  • Binding: Paperback
  • Language: English
  • Returnable: N
  • Weight: 54 gr


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