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Determinations of Atomic Weights Volume 125

Determinations of Atomic Weights Volume 125


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About the Book

This historic book may have numerous typos and missing text. Purchasers can download a free scanned copy of the original book (without typos) from the publisher. Not indexed. Not illustrated. 1910 edition. Excerpt: ... was being subjected to analysis in a series of experiments even more extended and careful than those concerning the bromide. In this case also it was a matter of very great importance to dry the salt thoroughly, and much time was spent in determining its properties upon heating. Some of the salt was dried in the air without fusion; some was fused in the air; some was fused in hydrochloric acid, and some was not fused at all, but the amount of anhydrous salt present was found by making a separate determination of the water in part of the same sample. In this way the weight of barium chloride corresponding to a definite weight of the crystallized salt was found with the greatest precision, and a sufficient basis was found for determining the precise weight of the anhydrous salt to be analyzed. At first an attempt was made to determine the ratio BaCl2: BaSO4, but the purity of even the best barium sulphate was found to be too uncertain to form the basis of any reliable conclusions. Accordingly, the determination of the halogen by combination with silver was again undertaken. This analysis was by no means so simple as in the case of the bromide. Stas in his early work ignored entirely the solubility of silver chloride, although this is sufficient to cause a very serious defect in any work pretending to accuracy. In his later work Stas devised methods for determining the end-point of the reaction of dissolved silver upon a soluble chloride, showing that by adding a sufficient excess of silver all the halogen could be precipitated. It seemed desirable, nevertheless, to confirm this knowledge, and accordingly new methods for accomplishing the end in question were devised and were used to verify Stas's methods, which were found to be approximately...


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Product Details
  • ISBN-13: 9780217131988
  • Publisher: Rarebooksclub.com
  • Publisher Imprint: Rarebooksclub.com
  • Height: 246 mm
  • No of Pages: 50
  • Spine Width: 3 mm
  • Width: 189 mm
  • ISBN-10: 0217131980
  • Publisher Date: 01 Jul 2012
  • Binding: Paperback
  • Language: English
  • Returnable: N
  • Weight: 109 gr


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