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A Manual of Etherization

A Manual of Etherization


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About the Book

This historic book may have numerous typos and missing text. Purchasers can download a free scanned copy of the original book (without typos) from the publisher. Not indexed. Not illustrated.1861 Excerpt: ... CHAPTER III. ETHER. Sulphuric Ether, or the Oxide of Ethyle, as it is now called, was known to the ancient chemists, and according to Berzelius, the first receipts for its preparation were published by Valerius Cordus, in 1540, who gave it the name of Oleum Vitrioli dulce. Basil, Valentine, and Paracelsus appear to have been acquainted with it, though not in its pure state. Frobenius gave the name Ether to this volatile liquid. It is prepared from a mixture of equal parts of alcohol, of specific gravity 0-830, and sulphuric acid of density 1-85 at 20 deg. Cent. The alcohol is first introduced into the retort, and while moving it so as to make it gyrate in it, the sulphuric acid is added in a small stream, and mixed thoroughly with the alcohol. The retort is then adapted to a voluminous tubulated recipient, the tubuluro- going into a bottle, and the retort is placed in a sand bath and distillation is effected at a moderate heat. At first considerable unaltered alcohol distils over; but when the proper temperature is reached, ether commences to distil. Peculiar striae appear in the neck of the retort, so long as ether is coming over; and when these cease the operation must be stopped. In this operation the sulphuric acid acts only by catalysis, aud is not itself decomposed; and since sulphuric acid forms no part of the ether, it is obvious that the name sulphuric ether is improper. V The best method of preparing ether, consists in running the alcohol in a small stream into acid, properly heated to the temperature required for the production of ether. If the acid has a specific gravity of 1-85 the reaction would be too violent, and the ether would be transformed into olefiant gas. It is necessary, therefore, to dilute the acid with water, until it is brou...


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Product Details
  • ISBN-13: 9780217073158
  • Publisher: General Books
  • Publisher Imprint: General Books
  • Height: 246 mm
  • No of Pages: 40
  • Spine Width: 2 mm
  • Width: 189 mm
  • ISBN-10: 0217073158
  • Publisher Date: 08 Feb 2012
  • Binding: Paperback
  • Language: English
  • Returnable: N
  • Weight: 91 gr


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