Methods of X-ray and Neutron Scattering in Polymer Science: (Topics in Polymer Science)

Methods of X-ray and Neutron Scattering in Polymer Science presents the basic theories underlying x-ray and neutron scattering--two of the most powerful tools for characterizing materials--and also covers the various techniques that have been developed for their application to the study of polymers. While there is a great deal of similarity between the x-ray and neutron scattering methods, the two were developed in different time periods by different groups of scientists, and as a result very distinct terminologies evolved to explain the same phenomena. In this unique text the two are presented together from the very beginning, with a consistent set of symbols and terminologies, so that students can become equally familiar with both from the outset. Also, to help students gain a unified view of diffraction, the distinction between wide-angle diffraction and small-angle scattering is postponed until late in the text. Methods of X-ray and Neutron Scattering in Polymer Science emphasizes basic concepts rather than details of specific techniques and derives relationships from first premises wherever possible. Beginning with coverage of the basic properties of x-rays and neutrons and their scattering from matter, it goes on to discuss methods of studying specific types of samples or properties. Topics covered include single-component crystalline and amorphous polymers; the small-angle scattering technique; binary, single-phase systems such as polymer blend and polymer solution; the technique of reflectivity measurement; and polymer dynamics by means of inelastic neutron scattering. A perfect introductory textbook for graduate and advanced undergraduate students in polymer science,Methods of X-ray and Neutron Scattering in Polymer Science also serves as a helpful self-study tool for polymer scientists seeking an introduction to scattering techniques. Further reading lists at the end of each chapter encourage readers to explore more advanced topics on their own.

Table of Contents:
1: Basics of X-ray and Neutron Scattering 1.1: Properties of X-rays and Neutrons 1.2: Scattering and Interference 1.3: Scattering of X-rays 1.4: Scattering of Neutrons 1.5: Auto-correlation Function and Reciprocal Space 1.6: Scattering Due to the Sample as a Whole 1.7: Diffraction by Crystals 2: Experimental Techniques 2.1: Radiation Source 2.2: Monochromatization 2.3: Absorption 2.4: Detectors 2.5: Cameras and Diffractometers 2.6: Multiple Scattering 2.7: Absolute Intensity Calibration 3: Crystalline Polymers 3.1: Introduction 3.2: Lattice Parameters 3.3: Crystal Structure Analysis 3.4: Line Broadening and Crystal Imperfections 3.5: Degree of Crystallinity 3.6: Orientation 4: Amorphous Polymers 4.1: Short Range Order 4.2: Thermal Density Fluctuation 5: Small Angle Scattering 5.1: Model Structures Studied by Small Angle Scattering 5.2: Dilute Particulate System 5.3: Non-particulate Two-phase system 5.4: Fractal Objects 5.5: Periodic System 5.6: Slit Collimation and Desmearing 6: Polymer Blends, Block Copolymers, and Deuterium Labeling 6.1: Polymer Blends 6.2: Block Copolymers 6.3: Deuterium Labeling 7: Methods of Study for Surfaces and Interfaces 7.1: Introduction 7.2: Reflectivity 7.3: Approximate Method 7.4: Examples of Experimental Studies 8: Inelastic Neutron Scattering 8.1: Theory of Inelastic Scattering 8.2: Simple Models of Motions 8.3: Spectrometers 8.4: Examples of Experimental Studies Appendix A: Refresher on Complex Numbers Appendix B: Fourier Transform Appendix C: Reciprocal Lattice Appendix D: Constants and Conversion Factors Glossary of Symbols

Review :
"Really excellent book! Already used by Roe for course in our Materials Science Department at the University of Cincinnati." --J.E. Mark, University of Cincinnati "This book covers all the essential topics and a host of advanced techniques in X-ray and neutron scattering. Useful both as a textbook and quick-reference." --George Skillas, University of Cincinnati