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Lessons in Qualitative and Volumetric Chemical Analysis; For the Use of Physicians, Pharmacists and Students

Lessons in Qualitative and Volumetric Chemical Analysis; For the Use of Physicians, Pharmacists and Students


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About the Book

This historic book may have numerous typos and missing text. Purchasers can download a free scanned copy of the original book (without typos) from the publisher. Not indexed. Not illustrated.1894 Excerpt: ... tube passes. The pipette is held in place in the long cylinder, E, by means of two notched disks of cork, F, F, and one between them of rubber, G, which permit raising and lowering the pipette, yet hold it firmly in any position. A short test-tube, B, (with mark at 4 Cc.) is also required, suitable to occupy the position within the bottle, A, as indicated in the figure. The solution of sodium hypobromite, which must be freshly prepared for each experiment, is made by adding 2.5 Cc. bromin to 47.5 Cc.of a 300 solution of Na0H. 0rdinary sodium hypochlorite (liquor soda? chloratae, U. S. P.) may also be employed, if mixed with solution of potassa. To insure complete absorption of the C02 it is best to add some Na0H or K0H to the water with which the cylinder, E, is filled. When a Lunge's nitrometer, fig. 35, is at hand, the bottle, A, may be attached to the outer tube of its three-way stop-cock, while the graduated tube is filled with Na0H solution. Example 31. Urea, C0(NH2)2. =59.95. Into the short test-tube B, put 4 Cc. of the urine to be examined and, by means of a pincette, place it carefully into position in the bottle A, previously filled with 15 Cc. of the sodium hypobromite solution (or with 15 Cc. of sodium hypochlorite, in which about 1 Gm. of K0H has been dissolved). Carefully close the bottle with the cork and connect with the pipette. This is adjusted in the cylinder filled with alkaline water, so that the level in both vessels corresponds with the zero mark of the pipette. Everything being thus prepared and air-tight closure of the joints being assured, the bottle, A, is now gently inclined, so that the contents of the tube, B, may flow out and mix with the hypobromite solution. As the reaction goes on the C02 is absorbed by the alkaline liquid, ...


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Product Details
  • ISBN-13: 9781150015915
  • Publisher: General Books
  • Publisher Imprint: General Books
  • Height: 246 mm
  • No of Pages: 112
  • Spine Width: 6 mm
  • Width: 189 mm
  • ISBN-10: 1150015918
  • Publisher Date: 09 Feb 2012
  • Binding: Paperback
  • Language: English
  • Returnable: N
  • Weight: 213 gr


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