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Manual of Qualitive Chemical Analysis

Manual of Qualitive Chemical Analysis


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This historic book may have numerous typos and missing text. Purchasers can download a free scanned copy of the original book (without typos) from the publisher. Not indexed. Not illustrated. 1883. Excerpt: ... of the stalks of cereals and others abounding in silicic acid that are not completely decomposed by H CL Boil the washed residue with solution of Naj C O3 in 278 excess, filter hot, wash with boiling water, and test for silicic acid in the nltrate by evaporation with H CI ( 150,2). If the ash was of a kind to be completely decomposed by H Cl, the analysis may be considered finished--for the accidental admixture of clay and sand will rarely interest the analyst sufficiently to warrant a more minute examination by fusing. But if the ash abounded in silicic acid, and it may therefore be supposed that the H CI has failed to effect complete decomposition, evaporate half of the residue insoluble in solution of Na2 C O3 with pure solution of Na O H in excess, in a silver or platinum dish, to dryness. This decomposes the silicates of the ash, whilst but little affecting the sand. Acidify now with H Cl, evaporate to dryness, etc., and proceed as in 275. For the detection of the alkalies use the other half of the residue, treating this according to 172. SECTION III. EXPLANATORY NOTES AND ADDITIONS TO THE SYSTEMATIC COURSE OF ANALYSIS. I. Additional Remarks To The Preliminary Examination. To 175-178. The inspection of the physical properties of a body may, as already stated, in many cases enable the analyst to draw certain general inferences as to its nature. Thus, for instance, if the analyst has a white substance before him, he may at once conclude that it is not cinnabar, or if a light substance, that it is not a compound of lead, etc. Inferences of this kind are quite admissible to a certain extent; but if carried too far, they are apt to mislead the operator, by blinding him to every reaction not exactly in accordance with his preconceived no...


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Product Details
  • ISBN-13: 9781150003493
  • Publisher: General Books
  • Publisher Imprint: General Books
  • Height: 246 mm
  • No of Pages: 186
  • Spine Width: 10 mm
  • Width: 189 mm
  • ISBN-10: 1150003499
  • Publisher Date: 01 Jan 2012
  • Binding: Paperback
  • Language: English
  • Returnable: N
  • Weight: 340 gr

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