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The Analyst Volume 26-27

The Analyst Volume 26-27


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This historic book may have numerous typos and missing text. Purchasers can download a free scanned copy of the original book (without typos) from the publisher. Not indexed. Not illustrated. 1900 Excerpt: ... does not induce a precipitate. Chromic salts are decomposed on continued boiling with sodium thiosulphate, yielding chromic hydroxide as in the equation: Cr2Cl6 + 3Na2S2O3 + 3H, O = Cr2O0H6 + 6NaCl + 3SO2 + Ss. As this method did not yield altogether satisfactory results, the precipitation was rendered more complete and rapid by adding to the solution of the chromic chloride a definite quantity of potassium chromate solution of known strength, together with some ammonium chloride, boiling, and deducting from the chromic oxide, obtained on igniting the precipitate, the amount due to the chromate added. Lead Salts.--Good results are given by the following method: The hot solution of lead nitrate is mixed with ammonium chloride, and the resulting precipitate of lead chloride allowed to dissolve in the hot liquid. On now adding a hot concentrated solution of sodium thiosulphate, the lead is precipitated quantitatively as sulphide. Mercuric Salts.--On treating a hot solution of mercuric chloride with sodium thiosulphate, the mercury is quantitatively precipitated as sulphide, and the precipitation is much more rapid than with hydrogen sulphide. Silver Salts.--These react at the ordinary temperature with sodium thiosulphate, yielding a white precipitate (Ag2S2O3), which on warming becomes yellow and finally black (Ag2S). The tabulated results given by the author show that the method is suitable for the quantitative estimation of silver. Nickel and Cobalt Salts.--Nickel salts give a black precipitate of nickel sulphide on being boiled with sodium thiosulphate, but too slowly and incompletely for a quantitative estimation, even after the addition of ammonium chloride. The same difficulty was experienced in the case of cobalt salts. C. A. M. The Seduction of Nitrate..


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Product Details
  • ISBN-13: 9781130169898
  • Publisher: Rarebooksclub.com
  • Publisher Imprint: Rarebooksclub.com
  • Height: 246 mm
  • No of Pages: 348
  • Spine Width: 18 mm
  • Width: 189 mm
  • ISBN-10: 1130169898
  • Publisher Date: 01 Mar 2012
  • Binding: Paperback
  • Language: English
  • Returnable: N
  • Weight: 621 gr


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