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Home > Science, Technology & Agriculture > Industrial chemistry and manufacturing technologies > Industrial chemistry and chemical engineering > Aspen Plus: Chemical Engineering Applications
Aspen Plus: Chemical Engineering Applications

Aspen Plus: Chemical Engineering Applications


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About the Book

Facilitates the process of learning and later mastering Aspen Plus® with step by step examples and succinct explanations Step-by-step textbook for identifying solutions to various process engineering problems via screenshots of the Aspen Plus® platforms in parallel with the related text Includes end-of-chapter problems and term project problems Includes online exam and quiz problems for instructors that are parametrized (i.e., adjustable) so that each student will have a standalone version Includes extra online material for students such as Aspen Plus®-related files that are used in the working tutorials throughout the entire textbook

Table of Contents:
Preface xvii The Book Theme xix About the Author xxi What Do You Get Out of This Book? xxiii Who Should Read This Book? xxv Notes for Instructors xxvii Acknowledgment xxix About the Companion Website xxxi 1 Introducing Aspen Plus 1 1.1 What Does Aspen Stand For? 1 1.2 What is Aspen Plus Process Simulation Model? 2 1.3 Launching Aspen Plus V8.8 3 1.4 Beginning a Simulation 4 1.5 Entering Components 14 1.6 Specifying the Property Method 15 1.7 Improvement of the Property Method Accuracy 23 1.8 File Saving 38 Exercise 1.1 40 1.9 A Good Flowsheeting Practice 40 1.10 Aspen Plus Built-In Help 40 1.11 For More Information 40 Homework/Classwork 1.1 (Pxy) 41 Homework/Classwork 1.2 (ΔGmix) 42 Homework/Classwork 1.3 (Likes Dissolve Likes) as Envisaged by NRTL Property Method 42 Homework/Classwork 1.4 (The Mixing Rule) 44 2 More on Aspen Plus Flowsheet Features (1) 49 2.1 Problem Description 49 2.2 Entering and Naming Compounds 49 2.3 Binary Interactions 51 2.4 The “Simulation” Environment: Activation Dashboard 53 2.5 Placing a Block and Material Stream from Model Palette 53 2.6 Block and Stream Manipulation 54 2.7 Data Input, Project Title, and Report Options 56 2.8 Running the Simulation 58 2.9 The Difference Among Recommended Property Methods 61 2.10 NIST/TDE Experimental Data 62 Homework/Classwork 2.1 (Water–Alcohol System) 65 Homework/Classwork 2.2 (Water–Acetone–EIPK System with NIST/DTE Data) 66 Homework/Classwork 2.3 (Water–Acetone–EIPK System Without NIST/DTE Data) 69 3 More on Aspen Plus Flowsheet Features (2) 71 3.1 Problem Description: Continuation to the Problem in Chapter 2 71 3.2 The Clean Parameters Step 71 3.3 Simulation Results Convergence 74 3.4 Adding Stream Table 76 3.5 Property Sets 78 3.6 Adding Stream Conditions 82 3.7 Printing from Aspen Plus 83 3.8 Viewing the Input Summary 84 3.9 Report Generation 85 3.10 Stream Properties 87 3.11 Adding a Flash Separation Unit 88 3.12 The Required Input for “Flash3”-Type Separator 90 3.13 Running the Simulation and Checking the Results 91 Homework/Classwork 3.1 (Output of Input Data and Results) 92 Homework/Classwork 3.2 (Output of Input Data and Results) 93 Homework/Classwork 3.3 (Output of Input Data and Results) 93 Homework/Classwork 3.4 (The Partition Coefficient of a Solute) 93 4 Flash Separation and Distillation Columns 99 4.1 Problem Description 99 4.2 Adding a Second Mixer and Flash 99 4.3 Design Specifications Study 101 Exercise 4.1 (Design Spec) 105 4.4 Aspen Plus Distillation Column Options 106 4.5 “DSTWU” Distillation Column 107 4.6 “Distl” Distillation Column 111 4.7 “RadFrac” Distillation Column 113 Homework/Classwork 4.1 (Water–Alcohol System) 120 Homework/Classwork 4.2 (Water–Acetone–EIPK System with NIST/DTE Data) 125 Homework/Classwork 4.3 (Water–Acetone–EIPK System Without NIST/DTE Data) 127 Homework/Classwork 4.4 (Scrubber) 128 5 Liquid–Liquid Extraction Process 131 5.1 Problem Description 131 5.2 The Proper Selection for Property Method for Extraction Processes 131 5.3 Defining New Property Sets 136 5.4 The Property Method Validation Versus Experimental Data Using Sensitivity Analysis 136 5.5 A Multistage Extraction Column 142 5.6 The Triangle Diagram 146 References 149 Homework/Classwork 5.1 (Separation of MEK from Octanol) 149 Homework/Classwork 5.2 (Separation of MEK from Water Using Octane) 150 Homework/Classwork 5.3 (Separation of Acetic Acid from Water Using Isopropyl Butyl Ether) 151 Homework/Classwork 5.4 (Separation of Acetone from Water Using Trichloroethane) 151 Homework/Classwork 5.5 (Separation of Propionic Acid from Water Using MEK) 152 6 Reactors with Simple Reaction Kinetic Forms 155 6.1 Problem Description 155 6.2 Defining Reaction Rate Constant to Aspen Plus® Environment 155 6.3 Entering Components and Method of Property 157 6.4 The Rigorous Plug-Flow Reactor (RPLUG) 159 6.5 Reactor and Reaction Specifications for RPLUG (PFR) 161 6.6 Running the Simulation (PFR Only) 167 Exercise 6.1 167 6.7 Compressor (CMPRSSR) and RadFrac Rectifying Column (RECTIF) 168 6.8 Running the Simulation (PFR + CMPRSSR + RECTIF) 171 Exercise 6.2 172 6.9 RadFrac Distillation Column (DSTL) 172 6.10 Running the Simulation (PFR + CMPRSSR + RECTIF + DSTL) 174 6.11 Reactor and Reaction Specifications for RCSTR 175 6.12 Running the Simulation (PFR + CMPRSSR + RECTIF + DSTL + RCSTR) 179 Exercise 6.3 180 6.13 Sensitivity Analysis: The Reactor’s Optimum Operating Conditions 181 References 188 Homework/Classwork 6.1 (Hydrogen Peroxide Shelf-Life) 189 Homework/Classwork 6.2 (Esterification Process) 192 Homework/Classwork 6.3 (Liquid-Phase Isomerization of n-Butane) 194 7 Reactors with Complex (Non-Conventional) Reaction Kinetic Forms 197 7.1 Problem Description 197 7.2 Non-Conventional Kinetics: LHHW Type Reaction 199 7.3 General Expressions for Specifying LHHW Type Reaction in Aspen Plus 200 7.3.1 The “Driving Force” for the Non-Reversible (Irreversible) Case 201 7.3.2 The “Driving Force” for the Reversible Case 201 7.3.3 The “Adsorption Expression” 202 7.4 The Property Method: “SRK” 202 7.5 Rplug Flowsheet for Methanol Production 203 7.6 Entering Input Parameters 203 7.7 Defining Methanol Production Reactions as LHHW Type 205 7.8 Sensitivity Analysis: Effect of Temperature and Pressure on Selectivity 216 References 219 Homework/Classwork 7.1 (Gas-Phase Oxidation of Chloroform) 220 Homework/Classwork 7.2 (Formation of Styrene from Ethylbenzene) 222 Homework/Classwork 7.3 (Combustion of Methane Over Steam-Aged Pt–Pd Catalyst) 225 8 Pressure Drop Friction Factor ANPSH and Cavitation 229 8.1 Problem Description 229 8.2 The Property Method: “STEAMNBS” 229 8.3 A Water Pumping Flowsheet 230 8.4 Entering Pipe, Pump, and Fittings Specifications 231 8.5 Results: Frictional Pressure Drop, the Pump Work, Valve Choking, and ANPSH Versus RNPSH 237 Exercise 8.1 238 8.6 Model Analysis Tools: Sensitivity for the Onset of Cavitation or Valve Choking Condition 242 References 247 Homework/Classwork 8.1 (Pentane Transport) 247 Homework/Classwork 8.2 (Glycerol Transport) 248 Homework/Classwork 8.3 (Air Compression) 249 9 The Optimization Tool 251 9.1 Problem Description: Defining the Objective Function 251 9.2 The Property Method: “STEAMNBS” 252 9.3 A Flowsheet for Water Transport 253 9.4 Entering Stream, Pump, and Pipe Specifications 253 9.5 Model Analysis Tools: The Optimization Tool 256 9.6 Model Analysis Tools: The Sensitivity Tool 260 9.7 Last Comments 263 References 264 Homework/Classwork 9.1 (Swamee–Jain Equation) 264 Homework/Classwork 9.2 (A Simplified Pipe Diameter Optimization) 264 Homework/Classwork 9.3 (The Optimum Diameter for a Viscous Flow) 265 Homework/Classwork 9.4 (The Selectivity of Parallel Reactions) 266 10 Heat Exchanger (H.E.) Design 269 10.1 Problem Description 269 10.2 Types of Heat Exchanger Models in Aspen Plus 270 10.3 The Simple Heat Exchanger Model (“Heater”) 272 10.4 The Rigorous Heat Exchanger Model (“HeatX”) 274 10.5 The Rigorous Exchanger Design and Rating (EDR) Procedure 279 10.5.1 The EDR Exchanger Feasibility Panel 279 10.5.2 The Rigorous Mode Within the “HeatX” Block 294 10.6 General Footnotes on EDR Exchanger 294 References 297 Homework/Classwork 10.1 (Heat Exchanger with Phase Change) 297 Homework/Classwork 10.2 (High Heat Duty Heat Exchanger) 298 Homework/Classwork 10.3 (Design Spec Heat Exchanger) 299 11 Electrolytes 301 11.1 Problem Description: Water De-Souring 301 11.2 What Is an Electrolyte? 301 11.3 The Property Method for Electrolytes 302 11.4 The Electrolyte Wizard 302 11.5 Water De-Souring Process Flowsheet 310 11.6 Entering the Specifications of Feed Streams and the Stripper 311 References 315 Homework/Classwork 11.1 (An Acidic Sludge Neutralization) 316 Homework/Classwork 11.2 (CO2 Removal from Natural Gas) 317 Homework/Classwork 11.3 (pH of Aqueous Solutions of Salts) 321 Appendix 11.A Development of “ELECNRTL” Model 324 12 Polymerization Processes 325 12.1 The Theoretical Background 325 12.1.1 Polymerization Reactions 325 12.1.2 Catalyst Types 326 12.1.3 Ethylene Process Types 327 12.1.4 Reaction Kinetic Scheme 327 12.1.5 Reaction Steps 327 12.1.6 Catalyst States 328 12.2 High-Density Polyethylene (HDPE) High-Temperature Solution Process 329 12.2.1 Problem Definition 330 12.2.2 Process Conditions 330 12.3 Creating Aspen Plus Flowsheet for HDPE 331 12.4 Improving Convergence 338 12.5 Presenting the Property Distribution of Polymer 339 References 343 Homework/Classwork 12.1 (Maximizing the Degree of HDPE Polymerization) 344 Homework/Classwork 12.2 (Styrene Acrylonitrile (SAN) Polymerization) 345 Appendix 12.A The Main Features and Assumptions of Aspen Plus Chain Polymerization Model 351 Appendix 12.A.1 Polymerization Mechanism 351 Appendix 12.A.2 Copolymerization Mechanism 351 Appendix 12.A.3 Rate Expressions 352 Appendix 12.A.4 Rate Constants 352 Appendix 12.A.5 Catalyst Preactivation 352 Appendix 12.A.6 Catalyst Site Activation 352 Appendix 12.A.7 Site Activation Reactions 353 Appendix 12.A.8 Chain Initiation 353 Appendix 12.A.9 Propagation 353 Appendix 12.A.10 Chain Transfer to Small Molecules 354 Appendix 12.A.11 Chain Transfer to Monomer 354 Appendix 12.A.12 Site Deactivation 354 Appendix 12.A.13 Site Inhibition 354 Appendix 12.A.14 Cocatalyst Poisoning 355 Appendix 12.A.15 Terminal Double Bond Polymerization 355 Appendix 12.A.16 Phase Equilibria 355 Appendix 12.A.17 Rate Calculations 355 Appendix 12.A.18 Calculated Polymer Properties 356 Appendix 12.B The Number Average Molecular Weight (MWN) and Weight Average Molecular Weight (MWW) 356 13 Characterization of Drug-Like Molecules Using Aspen Properties 361 13.1 Introduction 361 13.2 Problem Description 362 13.3 Creating Aspen Plus Pharmaceutical Template 363 13.3.1 Entering the User-Defined Benzamide (BNZMD-UD) as Conventional 363 13.3.2 Specifying Properties to Estimate 364 13.4 Defining Molecular Structure of BNZMD-UD 364 13.5 Entering Property Data 370 13.6 Contrasting Aspen Plus Databank (BNZMD-DB) Versus BNZMD-UD 373 References 375 Homework/Classwork 13.1 (Vanillin) 375 Homework/Classwork 13.2 (Ibuprofen) 376 14 Solids Handling 379 14.1 Introduction 379 14.2 Problem Description #1: The Crusher 379 14.3 Creating Aspen Plus Flowsheet 380 14.3.1 Entering Components Information 380 14.3.2 Adding the Flowsheet Objects 381 14.3.3 Defining the Particle Size Distribution (PSD) 382 14.3.4 Calculation of the Outlet PSD 385 Exercise 14.1 (Determine Crusher Outlet PSD from Comminution Power) 386 Exercise 14.2 (Specifying Crusher Outlet PSD) 386 14.4 Problem Description #2: The Fluidized Bed for Alumina Dehydration 387 14.5 Creating Aspen Plus Flowsheet 387 14.5.1 Entering Components Information 387 14.5.2 Adding the Flowsheet Objects 388 14.5.3 Entering Input Data 389 14.5.4 Results 391 Exercise 14.3 (Reconverging the Solution for an Input Change) 392 References 393 Homework/Classwork 14.1 (KCl Drying) 393 Homework/Classwork 14.2 (KCl Crystallization) 396 Appendix 14.A Solids Unit Operations 401 Appendix 14.A.1 Unit Operation Solids Models 401 Appendix 14.A.2 Solids Separators Models 401 Appendix 14.A.3 Solids Handling Models 402 Appendix 14.B Solids Classification 402 Appendix 14.C Predefined Stream Classification 403 Appendix 14.D Substream Classes 404 Appendix 14.E Particle Size Distribution (PSD) 405 Appendix 14.F Fluidized Beds 406 15 Aspen Plus® Dynamics 409 15.1 Introduction 409 15.2 Problem Description 410 15.3 Preparing Aspen Plus Simulation for Aspen Plus Dynamics (APD) 411 15.4 Conversion of Aspen Plus Steady-State into Dynamic Simulation 416 15.4.1 Modes of Dynamic CSTR Heat Transfer 417 15.4.2 Creating Pressure-Driven Dynamic Files for APD 422 15.5 Opening a Dynamic File Using APD 423 15.6 The “Simulation Messages” Window 424 15.7 The Running Mode: Initialization 425 15.8 Adding Temperature Control (TC) Unit 426 15.9 Snapshots Management for Captured Successful Old Runs 430 15.10 The Controller Faceplate 431 15.11 Communication Time for Updating/Presenting Results 434 15.12 The Closed-Loop Auto-Tune Variation (ATV) Test Versus Open-Loop Tune-Up Test 434 15.13 The Open-Loop (Manual Mode) Tune-Up for Liquid Level Controller 436 15.14 The Closed-Loop Dynamic Response for Liquid Level Load Disturbance 443 15.15 The Closed-Loop Dynamic Response for Liquid Level Set-Point Disturbance 448 15.16 Accounting for Dead/Lag Time in Process Dynamics 450 15.17 The Closed-Loop (Auto Mode) ATV Test for Temperature Controller (TC) 451 15.18 The Closed-Loop Dynamic Response: “TC” Response to Temperature Load Disturbance 459 15.19 Interactions Between “LC” and “TC” Control Unit 462 15.20 The Stability of a Process Without Control 464 15.21 The Cascade Control 466 15.22 Monitoring of Variables as Functions of Time 468 15.23 Final Notes on the Virtual (DRY) Process Control in APD 472 References 478 Homework/Classwork 15.1 (A Cascade Control of a Simple Water Heater) 478 Homework/Classwork 15.2 (A CSTR Control with “LMTD” Heat Transfer OPTION) 482 Homework/Classwork 15.3 (A PFR Control for Ethylbenzene Production) 483 16 Safety and Energy Aspects of Chemical Processes 487 16.1 Introduction 487 16.2 Problem Description 487 16.3 The “Safety Analysis” Environment 488 16.4 Adding a Pressure Safety Valve (PSV) 490 16.5 Adding a Rupture Disk (RD) 496 16.6 Presentation of Safety-Related Documents 500 16.7 Preparation of Flowsheet for “Energy Analysis” Environment 501 16.8 The “Energy Analysis” Activation 506 16.9 The “Energy Analysis” Environment 510 16.10 The Aspen Energy Analyzer 512 Homework/Classwork 16.1 (Adding a Storage Tank Protection) 513 Homework/Classwork 16.2 (Separation of C2/C3/C4 Hydrocarbon Mixture) 518 17 Aspen Process Economic Analyzer (APEA) 523 17.1 Optimized Process Flowsheet for Acetic Anhydride Production 523 17.2 Costing Options in Aspen Plus 525 17.2.1 Aspen Process Economic Analyzer (APEA) Estimation Template 525 17.2.2 Feed and Product Stream Prices 527 17.2.3 Utility Association with a Flowsheet Block 528 17.3 The First Route for Chemical Process Costing 531 17.4 The Second Round for Chemical Process Costing 532 17.4.1 Project Properties 533 17.4.2 Loading Simulator Data 535 17.4.3 Mapping and Sizing 537 17.4.4 Project Evaluation 544 17.4.5 Fixing Geometrical Design-Related Errors 546 17.4.6 Executive Summary 549 17.4.7 Capital Costs Report 550 17.4.8 Investment Analysis 551 Homework/Classwork 17.1 (Feed/Product Unit Price Effect on Process Profitability) 555 Homework/Classwork 17.2 (Using European Economic Template) 556 Homework/Classwork 17.3 (Process Profitability of Acetone Recovery from Spent Solvent) 556 Appendix 17.A 559 Appendix 17.A.1 Net Present Value (NPV) for a Chemical Process Plant 559 Appendix 17.A.2 Discounted Payout (PAYBACK) Period (DPP) 560 Example 17.1 (Uniform Cash Flow) 561 Example 17.2 (Non-Uniform Cash Flow) 561 Appendix 17.A.3 Profitability Index 561 Example 17.3 562 Appendix 17.A.4 Internal Rate of Return (IRR) 562 Appendix 17.A.5 Modified Internal Rate of Return (MIRR) 563 Example 17.4 563 18 Term Projects (TP) 565 18.1 TP #1: Production of Acetone via the Dehydration of Isopropanol 565 18.2 TP #2: Production of Formaldehyde from Methanol (Sensitivity Analysis) 569 18.3 TP #3: Production of Dimethyl Ether (Process Economics and Control) 570 18.3.1 Economic Analysis 570 18.3.2 Process Dynamics and Control 572 18.4 TP #4: Production of Acetic Acid via Partial Oxidation of Ethylene Gas 574 18.5 TP #5: Pyrolysis of Benzene 575 18.6 TP #6: Reuse of Spent Solvents 575 18.7 TP #7: Solids Handling: Production of Potassium Sulfate from Sodium Sulfate 576 18.8 TP #8: Solids Handling: Production of CaCO3-Based Agglomerate as a General Additive 577 18.9 TP #9: Solids Handling: Formulation of Di-Ammonium Phosphate and Potassium Nitrate Blend Fertilizer 577 18.10 TP #10: “Flowsheeting Options” | “Calculator”: Gas De-Souring and Sweetening Process 578 18.11 TP #11: Using More than One Property Method and Stream Class: Solid Catalyzed Direct Hydration of Propylene to Isopropyl Alcohol (IPA) 582 18.12 TP #12: Polymerization: Production of Polyvinyl Acetate (PVAC) 586 18.13 TP #13: Polymerization: Emulsion Copolymerization of Styrene and Butadiene to Produce SBR 588 18.14 TP #14: Polymerization: Free Radical Polymerization of Methyl Methacrylate to Produce Poly(Methyl Methacrylate) 590 18.15 TP #15: LHHW Kinetics: Production of Cyclohexanone-Oxime (CYCHXOXM) via Cyclohexanone Ammoximation Using Clay-Based Titanium Silicalite (TS) Catalyst 592 Index 595

About the Author :
Kamal Al-Malah, is professor of chemical engineering at Higher Colleges of Technology, United Arab Emirates and former chairman of the chemical engineering department at the University of Hail in Saudi Arabia. He holds B.S., M.S., and Ph.D. degrees in chemical/biochemical engineering. Dr. Al-Malah graduated from Oregon State University in 1993 and his area of specialty deals with mathematical modeling, optimization, simulation, and computer-aided design. Professor Al-Malah is Windows-based software developer and MATLAB® book author


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Product Details
  • ISBN-13: 9781119293644
  • Publisher: John Wiley & Sons Inc
  • Publisher Imprint: John Wiley & Sons Inc
  • Height: 250 mm
  • No of Pages: 656
  • Sub Title: Chemical Engineering Applications
  • Width: 150 mm
  • ISBN-10: 1119293642
  • Publisher Date: 26 Sep 2016
  • Binding: Digital online
  • Language: English
  • Spine Width: 15 mm
  • Weight: 666 gr


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